N-{2-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2-yl]-ethyl}-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-{2-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2-yl]-ethyl}-4-methyl-benzenesulfonamide
CAS No.:914662-15-0
Molecular Formula:C₂₂H₂₅NO₄S
Molecular Weight:399.511
Hs Code.:

Synonyms:N-{2-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2-yl]-ethyl}-4-methyl-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{2-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2-yl]-ethyl}-4-methyl-benzenesulfonamide

Chemical Property:

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Technology Process of N-{2-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2-yl]-ethyl}-4-methyl-benzenesulfonamide

There total 6 articles about N-{2-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2-yl]-ethyl}-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2-yl]-ethylamine

: 98-59-9
p-toluenesulfonyl chloride

: 914662-15-0
N-{2-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2-yl]-ethyl}-4-methyl-benzenesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1002/chem.200600533

Reference yield:

: 914661-74-8
2-(4-methoxy-2,6-dimethyl-phenyl)-furan

: 914662-15-0
N-{2-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2-yl]-ethyl}-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / phosphorus oxychloride / 12 h / 40 °C

2: 59 percent / potassium hydroxide / methanol / 0 - 20 °C

3: lithium aluminum anhydride / diethyl ether / 16 h / Heating

4: 50 mg / triethylamine / CH₂Cl₂ / 12 h / 20 °C

With potassium hydroxide; lithium aluminium tetrahydride; triethylamine; trichlorophosphate; In methanol; diethyl ether; dichloromethane; 1: Vilsmeier-Haack reaction;
DOI:10.1002/chem.200600533

Reference yield:

: 914661-57-7
1-(4-methoxy-2,6-dimethyl-phenyl)-but-3-yn-1-ol

: 914662-15-0
N-{2-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2-yl]-ethyl}-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1: 83 percent / Dess-Martin periodinane / CH₂Cl₂ / 20 °C

2: 78 percent / silver nitrate / acetone / 12 h / 20 °C

3: 96 percent / phosphorus oxychloride / 12 h / 40 °C

4: 59 percent / potassium hydroxide / methanol / 0 - 20 °C

5: lithium aluminum anhydride / diethyl ether / 16 h / Heating

6: 50 mg / triethylamine / CH₂Cl₂ / 12 h / 20 °C

With potassium hydroxide; lithium aluminium tetrahydride; Dess-Martin periodane; silver nitrate; triethylamine; trichlorophosphate; In methanol; diethyl ether; dichloromethane; acetone; 1: Dess-Martin oxidation / 3: Vilsmeier-Haack reaction;
DOI:10.1002/chem.200600533