4,4-difluoro-8-[3,4-bis(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxymethyl}propoxy)phenyl]-1,3,5,7-tetramethyl-2,6-diiodo-4-bora-3a,4a-diaza-s-indacene

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Chemical Name:4,4-difluoro-8-[3,4-bis(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxymethyl}propoxy)phenyl]-1,3,5,7-tetramethyl-2,6-diiodo-4-bora-3a,4a-diaza-s-indacene
CAS No.:1259292-37-9
Molecular Formula:C₅₅H₈₉BF₂I₂N₂O₁₈
Molecular Weight:1368.93
Hs Code.:

4,4-difluoro-8-[3,4-bis(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxymethyl}propoxy)phenyl]-1,3,5,7-tetramethyl-2,6-diiodo-4-bora-3a,4a-diaza-s-indacene

Synonyms:4,4-difluoro-8-[3,4-bis(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxymethyl}propoxy)phenyl]-1,3,5,7-tetramethyl-2,6-diiodo-4-bora-3a,4a-diaza-s-indacene

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Chemical Property of 4,4-difluoro-8-[3,4-bis(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxymethyl}propoxy)phenyl]-1,3,5,7-tetramethyl-2,6-diiodo-4-bora-3a,4a-diaza-s-indacene

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Technology Process of 4,4-difluoro-8-[3,4-bis(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxymethyl}propoxy)phenyl]-1,3,5,7-tetramethyl-2,6-diiodo-4-bora-3a,4a-diaza-s-indacene

There total 7 articles about 4,4-difluoro-8-[3,4-bis(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxymethyl}propoxy)phenyl]-1,3,5,7-tetramethyl-2,6-diiodo-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1259292-35-7
4,4-difluoro-8-[3,4-bis(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxymethyl}propoxy)phenyl]-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

: 1259292-37-9
4,4-difluoro-8-[3,4-bis(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxymethyl}propoxy)phenyl]-1,3,5,7-tetramethyl-2,6-diiodo-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: With iodine; iodic acid; In ethanol; water; at 40 ℃; for 0.075h;
DOI:10.1021/ol102758z

Reference yield:

: 1259292-32-4
3,4-bis(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxymethyl}propoxy)benzaldehyde

: 1259292-37-9
4,4-difluoro-8-[3,4-bis(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxymethyl}propoxy)phenyl]-1,3,5,7-tetramethyl-2,6-diiodo-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 12 h / 20 °C / Inert atmosphere; Darkness

1.2: 0.67 h / Inert atmosphere

2.1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.67 h / Inert atmosphere

3.1: iodine; iodic acid / ethanol; water / 0.07 h / 40 °C

With boron trifluoride diethyl etherate; iodine; iodic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In ethanol; dichloromethane; water;
DOI:10.1021/ol102758z

Reference yield:

: 1259292-31-3
2-bromomethyl-1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propane

: 1259292-37-9
4,4-difluoro-8-[3,4-bis(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxymethyl}propoxy)phenyl]-1,3,5,7-tetramethyl-2,6-diiodo-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 80 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 12 h / 20 °C / Inert atmosphere; Darkness

2.2: 0.67 h / Inert atmosphere

3.1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.67 h / Inert atmosphere

4.1: iodine; iodic acid / ethanol; water / 0.07 h / 40 °C

With boron trifluoride diethyl etherate; iodine; iodic acid; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol102758z