2-(4-methoxy-3,5-dimethylphenyl)phenanthren-4-ol

Base Information

Chemical Name:2-(4-methoxy-3,5-dimethylphenyl)phenanthren-4-ol
CAS No.:1612866-63-3
Molecular Formula:C₂₃H₂₀O₂
Molecular Weight:328.411
Hs Code.:

Synonyms:2-(4-methoxy-3,5-dimethylphenyl)phenanthren-4-ol

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Chemical Property of 2-(4-methoxy-3,5-dimethylphenyl)phenanthren-4-ol

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Technology Process of 2-(4-methoxy-3,5-dimethylphenyl)phenanthren-4-ol

There total 5 articles about 2-(4-methoxy-3,5-dimethylphenyl)phenanthren-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55215-54-8
5-iodo-2-methoxy-1,3-dimethylbenzene

: 1612866-63-3
2-(4-methoxy-3,5-dimethylphenyl)phenanthren-4-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 0.08 h / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 20 °C

3.1: 2-Methylpropionic anhydride / 48 h / 190 °C / Inert atmosphere

3.2: 60 - 100 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 2-Methylpropionic anhydride; potassium carbonate; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1002/anie.201310491

Reference yield:

: 14804-38-7
5-bromo-2-methoxy-1,3-dimethylbenzene

: 1612866-63-3
2-(4-methoxy-3,5-dimethylphenyl)phenanthren-4-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: tert.-butyl lithium / hexane; diethyl ether / 1 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 - 20 °C / Inert atmosphere

2.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 0.08 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: potassium carbonate / methanol / 20 °C

4.1: 2-Methylpropionic anhydride / 48 h / 190 °C / Inert atmosphere

4.2: 60 - 100 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tert.-butyl lithium; 2-Methylpropionic anhydride; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; diethyl ether; hexane;
DOI:10.1002/anie.201310491

Reference yield:

: C₁₄H₂₀OSi

: 1612866-63-3
2-(4-methoxy-3,5-dimethylphenyl)phenanthren-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / methanol / 20 °C

2.1: 2-Methylpropionic anhydride / 48 h / 190 °C / Inert atmosphere

2.2: 60 - 100 °C

With 2-Methylpropionic anhydride; potassium carbonate; In methanol;
DOI:10.1002/anie.201310491