{Pd₂CoI(CO)3(dppm)2}

Base Information

Chemical Name:{Pd₂CoI(CO)3(dppm)2}
CAS No.:113109-28-7
Molecular Formula:C₅₃H₄₄CoIO₃P₄Pd₂
Molecular Weight:1251.56
Hs Code.:

Synonyms:{Pd₂CoI(CO)3(dppm)2}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {Pd₂CoI(CO)3(dppm)2}

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Technology Process of {Pd₂CoI(CO)3(dppm)2}

There total 6 articles about {Pd₂CoI(CO)3(dppm)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 113109-24-3
{Pd₂Co₂(CO)7(dppm)2}

: 113109-28-7
{Pd₂CoI(CO)3(dppm)2}

Guidance literature:: With KI; In water; acetone; byproducts: K{Co(CO)4}; A soln. of KI in a mixt. of acetone and H2O was added to a soln. of {Pd2Co2(CO)7(dppm)2} in acetone.; After 1 h, n-hexane was added and the resulting ppt. was filtered off and dried. Purifn. was achieved by dissolving this solid in toluene and filtering the soln. Addn. of n-hexane afforded a powder. Elem.anal.;

Reference yield: 51.0%

: 113109-24-3
{Pd₂Co₂(CO)7(dppm)2}

: 68-05-3
tetraethylammonium iodide

: 113109-28-7
{Pd₂CoI(CO)3(dppm)2}

: 29477-07-4
{NEt₄}{Co(CO)4}

Guidance literature:: In dichloromethane; A soln. of {NEt4}I in CH2Cl2 was added to a soln. of {Pd2Co2(CO)7(dppm)2} in CH2Cl2.; Addn. of n-C6H14 to the soln. and cooling (-20°C) gave a ppt. of {NEt4}I (removed by filtration). More n-C6H14 was then added to the soln. and afforded a powder contg. {NEt4}{Co(CO)4} and {Pd2Co(CO)3(dppm)2I} (fractional crystn.).;