C₂₂H₂₅NO₃S

Base Information

Chemical Name:C₂₂H₂₅NO₃S
CAS No.:1334535-40-8
Molecular Formula:C₂₂H₂₅NO₃S
Molecular Weight:383.511
Hs Code.:

C<sub>22</sub>H<sub>25</sub>NO<sub>3</sub>S

Synonyms:C₂₂H₂₅NO₃S

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Chemical Property of C₂₂H₂₅NO₃S

Chemical Property:

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Technology Process of C₂₂H₂₅NO₃S

There total 3 articles about C₂₂H₂₅NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1334535-39-5
C₂₂H₂₄N₂O₂S

: 1334535-40-8
C₂₂H₂₅NO₃S

Guidance literature:: C₂₂H₂₄N₂O₂S; With hydrogenchloride; sodium nitrite; In water; at 60 ℃; for 2.5h; Inert atmosphere;

With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h; optical yield given as %ee;
DOI:10.1002/anie.201103937

Reference yield:

: 1334535-03-3
N-allyl-N-[2-(1H-indol-3-yl)ethyl]-4-methylbenzenesulfonamide

: 1334535-40-8
C₂₂H₂₅NO₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / 1,2-dichloro-ethane / 48 h / 60 °C / Inert atmosphere

2.1: 9-epi-9-amino-9-deoxyquinine; ortho-nitrobenzoic acid / 1,4-dioxane / 48 h / 20 °C / Inert atmosphere

3.1: sodium; hydrazine hydrate / ethylene glycol / 3 h / 190 °C / Inert atmosphere

4.1: potassium permanganate; 18-crown-6 ether / benzene / 20 °C / Inert atmosphere

5.1: hydrogenchloride; sodium nitrite / water / 2.5 h / 60 °C / Inert atmosphere

5.2: 0.5 h / 20 °C

With 9-epi-9-amino-9-deoxyquinine; hydrogenchloride; potassium permanganate; 18-crown-6 ether; 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride; ortho-nitrobenzoic acid; sodium; hydrazine hydrate; sodium nitrite; In 1,4-dioxane; water; ethylene glycol; 1,2-dichloro-ethane; benzene; 3.1: Huang Minlong reduction reaction;
DOI:10.1002/anie.201103937

Reference yield:

: 1334535-24-8
(4aR,7aR,12bR)-3-tosyl-1,2,3,4,4a,5,7a,8-octahydropyrido[3,4-d]carbazol-6(7H)-one

: 1334535-40-8
C₂₂H₂₅NO₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium; hydrazine hydrate / ethylene glycol / 3 h / 190 °C / Inert atmosphere

2.1: potassium permanganate; 18-crown-6 ether / benzene / 20 °C / Inert atmosphere

3.1: hydrogenchloride; sodium nitrite / water / 2.5 h / 60 °C / Inert atmosphere

3.2: 0.5 h / 20 °C

With hydrogenchloride; potassium permanganate; 18-crown-6 ether; sodium; hydrazine hydrate; sodium nitrite; In water; ethylene glycol; benzene; 1.1: Huang Minlong reduction reaction;
DOI:10.1002/anie.201103937