1D-2-acetamido-1,3,4,5-tetra-O-acetyl-2-deoxy-6-O-methyl-chiro-inositol

Base Information

Chemical Name:1D-2-acetamido-1,3,4,5-tetra-O-acetyl-2-deoxy-6-O-methyl-chiro-inositol
CAS No.:134235-55-5
Molecular Formula:C₁₇H₂₅NO₁₀
Molecular Weight:403.386
Hs Code.:

Synonyms:1D-2-acetamido-1,3,4,5-tetra-O-acetyl-2-deoxy-6-O-methyl-chiro-inositol

Suppliers and Price of 1D-2-acetamido-1,3,4,5-tetra-O-acetyl-2-deoxy-6-O-methyl-chiro-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1D-2-acetamido-1,3,4,5-tetra-O-acetyl-2-deoxy-6-O-methyl-chiro-inositol

Chemical Property:

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Technology Process of 1D-2-acetamido-1,3,4,5-tetra-O-acetyl-2-deoxy-6-O-methyl-chiro-inositol

There total 7 articles about 1D-2-acetamido-1,3,4,5-tetra-O-acetyl-2-deoxy-6-O-methyl-chiro-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 108-24-7
acetic anhydride

: 134235-54-4
1D-1,3,4,5-tetra-O-acetyl-2-azido-2-deoxy-6-O-methyl-chiro-inositol

: 134235-55-5
1D-2-acetamido-1,3,4,5-tetra-O-acetyl-2-deoxy-6-O-methyl-chiro-inositol

Guidance literature:: With hydrogen; Raney nickel T-4; In ethanol; under 760 Torr; Ambient temperature;
DOI:10.1016/0008-6215(91)80116-5

Reference yield:

: 642-38-6
quebrachitol

: 134235-55-5
1D-2-acetamido-1,3,4,5-tetra-O-acetyl-2-deoxy-6-O-methyl-chiro-inositol

Guidance literature:: Multi-step reaction with 7 steps

1: 6.9 g / p-toluenesulfonic acid monohydrate / dimethylformamide / 16 h / Ambient temperature

2: pyridine / 26 h / Ambient temperature

3: 80percent aq. HOAc / 4 h / Ambient temperature

4: 1.) pyridine, 2.) 80percent aq. HOAc / 1.) RT, 20 h, 2.) 50 deg C, 16 h

5: 84 percent / pyridine

6: 43 percent / NaN₃ / 2-methoxy-ethanol; H₂O / 20 h / Heating

7: 60 percent / H₂ / Raney nickel T-4 / ethanol / 760 Torr / Ambient temperature

With pyridine; sodium azide; hydrogen; toluene-4-sulfonic acid; acetic acid; Raney nickel T-4; In ethanol; 2-methoxy-ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(91)80116-5

Reference yield:

: 58769-23-6
1L-3,4,:5,6-di-O-isopropylidene-2-O-methyl-chiro-inositol

: 134235-55-5
1D-2-acetamido-1,3,4,5-tetra-O-acetyl-2-deoxy-6-O-methyl-chiro-inositol

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / 26 h / Ambient temperature

2: 80percent aq. HOAc / 4 h / Ambient temperature

3: 1.) pyridine, 2.) 80percent aq. HOAc / 1.) RT, 20 h, 2.) 50 deg C, 16 h

4: 84 percent / pyridine

5: 43 percent / NaN₃ / 2-methoxy-ethanol; H₂O / 20 h / Heating

6: 60 percent / H₂ / Raney nickel T-4 / ethanol / 760 Torr / Ambient temperature

With pyridine; sodium azide; hydrogen; acetic acid; Raney nickel T-4; In ethanol; 2-methoxy-ethanol; water;
DOI:10.1016/0008-6215(91)80116-5