(4α,4aα,8aβ)-4-(4-chlorophenyl)-4a,5,6,7,8,8a-hexahydro-8a-hydroxy-4H-3,1-benzothiazine-2(1H)-thione

Base Information

Chemical Name:(4α,4aα,8aβ)-4-(4-chlorophenyl)-4a,5,6,7,8,8a-hexahydro-8a-hydroxy-4H-3,1-benzothiazine-2(1H)-thione
CAS No.:118227-93-3
Molecular Formula:C₁₄H₁₆ClNOS₂
Molecular Weight:313.872
Hs Code.:

Synonyms:(4α,4aα,8aβ)-4-(4-chlorophenyl)-4a,5,6,7,8,8a-hexahydro-8a-hydroxy-4H-3,1-benzothiazine-2(1H)-thione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4α,4aα,8aβ)-4-(4-chlorophenyl)-4a,5,6,7,8,8a-hexahydro-8a-hydroxy-4H-3,1-benzothiazine-2(1H)-thione

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Technology Process of (4α,4aα,8aβ)-4-(4-chlorophenyl)-4a,5,6,7,8,8a-hexahydro-8a-hydroxy-4H-3,1-benzothiazine-2(1H)-thione

There total 2 articles about (4α,4aα,8aβ)-4-(4-chlorophenyl)-4a,5,6,7,8,8a-hexahydro-8a-hydroxy-4H-3,1-benzothiazine-2(1H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 31021-05-3
(E)-2-(4-chlorobenzylidene)cyclohexanone

: 513-74-6
ammonium dithiocarbamate

: 118227-93-3
(4α,4aα,8aβ)-4-(4-chlorophenyl)-4a,5,6,7,8,8a-hexahydro-8a-hydroxy-4H-3,1-benzothiazine-2(1H)-thione

Guidance literature:: With hydrogenchloride; In methanol; water; acetone; at -5 ℃; for 4h;

Reference yield:

: 31021-05-3
(E)-2-(4-chlorobenzylidene)cyclohexanone

: 513-74-6
ammonium dithiocarbamate

: 118227-93-3
(4α,4aα,8aβ)-4-(4-chlorophenyl)-4a,5,6,7,8,8a-hexahydro-8a-hydroxy-4H-3,1-benzothiazine-2(1H)-thione

: 118332-75-5
(4R,4aR,8aR)-4-(4-Chloro-phenyl)-8a-hydroxy-octahydro-benzo[d][1,3]thiazine-2-thione

Guidance literature:: With hydrogenchloride; In methanol; water; at -5 ℃; for 4h; Product distribution; further time and various concentration of reagent;