ethyl (2R,3S)-2-((bis(4-methoxy-3,5-dimethylphenyl)methyl)amino)-3-hydroxyoctadecanoate

Base Information

Chemical Name:ethyl (2R,3S)-2-((bis(4-methoxy-3,5-dimethylphenyl)methyl)amino)-3-hydroxyoctadecanoate
CAS No.:1606993-85-4
Molecular Formula:C₃₉H₆₃NO₅
Molecular Weight:625.933
Hs Code.:

Synonyms:ethyl (2R,3S)-2-((bis(4-methoxy-3,5-dimethylphenyl)methyl)amino)-3-hydroxyoctadecanoate

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Chemical Property of ethyl (2R,3S)-2-((bis(4-methoxy-3,5-dimethylphenyl)methyl)amino)-3-hydroxyoctadecanoate

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Technology Process of ethyl (2R,3S)-2-((bis(4-methoxy-3,5-dimethylphenyl)methyl)amino)-3-hydroxyoctadecanoate

There total 6 articles about ethyl (2R,3S)-2-((bis(4-methoxy-3,5-dimethylphenyl)methyl)amino)-3-hydroxyoctadecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1338801-11-8
(2R,3R)-ethyl 1-(bis(4-methoxy-3,5-dimethylphenyl)methyl)-3-pentadecylaziridine-2-carboxylate

: 1606993-85-4
ethyl (2R,3S)-2-((bis(4-methoxy-3,5-dimethylphenyl)methyl)amino)-3-hydroxyoctadecanoate

Guidance literature:: (2R,3R)-ethyl 1-(bis(4-methoxy-3,5-dimethylphenyl)methyl)-3-pentadecylaziridine-2-carboxylate; With trifluoroacetic acid; In dichloromethane; at 25 ℃; for 48h; Inert atmosphere;

With sodium hydroxide; In ethanol; water; at 20 ℃; for 0.333333h;
DOI:10.1002/ejoc.201301766

Reference yield:

: 629-80-1
n-hexadecylaldehyde

: 1606993-85-4
ethyl (2R,3S)-2-((bis(4-methoxy-3,5-dimethylphenyl)methyl)amino)-3-hydroxyoctadecanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: (2S)-(-)-3,3'-diphenyl-(2,2'-binaphthalene)-1,1'-diol; triphenylborane / toluene / 0.5 h / 80 °C / Inert atmosphere; Schlenk technique

1.2: 24 h / -10 °C / Molecular sieve; Inert atmosphere; Schlenk technique

2.1: dichloromethane / 48 h / 25 °C / Inert atmosphere

3.1: sodium hydroxide / ethanol; water / 0.33 h / 20 °C / Inert atmosphere

With triphenylborane; sodium hydroxide; (2S)-(-)-3,3'-diphenyl-(2,2'-binaphthalene)-1,1'-diol; In ethanol; dichloromethane; water; toluene;
DOI:10.1002/ejoc.201301766