methyl 3,5-bis{3',4',5'-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyloxy}benzoate

Base Information

• Chemical Name: methyl 3,5-bis{3',4',5'-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyloxy}benzoate
• CAS No.: 331822-38-9
• Molecular Formula: C₁₃₆H₂₀₀O₁₆
• Molecular Weight: 2091.07

Synonyms:methyl 3,5-bis{3',4',5'-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyloxy}benzoate

Chemical Property of methyl 3,5-bis{3',4',5'-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyloxy}benzoate

Chemical Property:

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Technology Process of methyl 3,5-bis{3',4',5'-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyloxy}benzoate

There total 2 articles about methyl 3,5-bis{3',4',5'-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyloxy}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.6%

1-carbomethoxy-3,5-dihydroxybenzene (2150-44-9) + 3,4,5-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyl chloride (331822-25-4) → methyl 3,5-bis{3',4',5'-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyloxy}benzoate (331822-38-9)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; at 70 ℃; for 4h;

DOI:10.1021/ja0037771

Reference yield: 43.0%

1-carbomethoxy-3,5-dihydroxybenzene (2150-44-9) + 3,4,5-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyl alcohol (161401-95-2) → methyl 3,5-bis{3',4',5'-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyloxy}benzoate (331822-38-9)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1002/anie.200800164

Reference yield: 90.2%

methyl 3,5-bis{3',4',5'-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyloxy}benzoate (331822-38-9) → 3,5-bis{3',4',5'-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyloxy}benzyl alcohol

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1021/ja0037771

upstream raw materials:

1-carbomethoxy-3,5-dihydroxybenzene

3,4,5-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyl chloride

3,4,5-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyl alcohol

Downstream raw materials:

3,5-bis{3',4',5'-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyloxy}benzoic acid

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