[2-(Me₂NCH₂)C₆H₄]PhSnCl₂

Base Information

• Chemical Name: [2-(Me₂NCH₂)C₆H₄]PhSnCl₂
• CAS No.: 72211-09-7
• Molecular Formula: C₁₅H₁₇Cl₂NSn
• Molecular Weight: 400.923
• Mol file: 72211-09-7.mol

Synonyms:[2-(Me₂NCH₂)C₆H₄]PhSnCl₂

Chemical Property of [2-(Me₂NCH₂)C₆H₄]PhSnCl₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [2-(Me₂NCH₂)C₆H₄]PhSnCl₂

There total 1 articles about [2-(Me₂NCH₂)C₆H₄]PhSnCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-(N,N-dimethylaminomethyl)phenyl)Ph2SnCl*HCl (1256962-54-5) → [2-(N,N-dimethylaminomethyl)phenyl]diphenyltin(IV) chloride (342371-85-1) + [2-(Me2NCH2)C6H4]PhSnCl2 (72211-09-7)

Guidance literature:

In neat (no solvent); byproducts: C6H6, HCl; heating in an open vessel at 10°C/min; not isolated, detected by NMR;

DOI:10.1016/j.jorganchem.2010.08.006

Reference yield: 89.0%

[2-(Me2NCH2)C6H4]PhSnCl2 (72211-09-7) + silver nitrate → C15H17N3O6Sn

Guidance literature:

In acetonitrile; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jorganchem.2017.03.019

Reference yield: 73.0%

hydrogenchloride (7647-01-0,15364-23-5) + [2-(Me2NCH2)C6H4]PhSnCl2 (72211-09-7) → (2-(N,N-dimethylaminomethyl)phenyl)PhSnCl2*HCl (1256962-63-6)

Guidance literature:

In tetrahydrofuran; diethyl ether; water; aq. HCl added to a soln. of Sn complex in THF/Et2O, stirred overnight; evapd. (vac.), extd. (CHCl3), concd. (vac.); elem. anal.;

DOI:10.1016/j.jorganchem.2010.08.006

upstream raw materials:

(2-(N,N-dimethylaminomethyl)phenyl)Ph₂SnCl*HCl

Downstream raw materials:

(2-(N,N-dimethylaminomethyl)phenyl)PhSnCl₂*HCl

[(2-(N,N-dimethylaminomethyl)phenyl)Sn(Ph)(trifluoroacetate)2]

[(2-(N,N-dimethylaminomethyl)phenyl)tin(IV)(phenyl)(trifluoromethanesulfonate)2]