C₁₉H₂₆FN₃O₅S

Base Information

Chemical Name:C₁₉H₂₆FN₃O₅S
CAS No.:1616109-94-4
Molecular Formula:C₁₉H₂₆FN₃O₅S
Molecular Weight:427.497
Hs Code.:

C<sub>19</sub>H<sub>26</sub>FN<sub>3</sub>O<sub>5</sub>S

Synonyms:C₁₉H₂₆FN₃O₅S

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Chemical Property of C₁₉H₂₆FN₃O₅S

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Technology Process of C₁₉H₂₆FN₃O₅S

There total 9 articles about C₁₉H₂₆FN₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616109-92-2
C₁₉H₂₄FN₃O₇S

: 1616109-94-4
C₁₉H₂₆FN₃O₅S

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 40 ℃; for 3h;

Reference yield:

: 1402742-12-4
C₁₉H₂₂FNO₂S

: 1616109-94-4
C₁₉H₂₆FN₃O₅S

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 3 h / -78 °C

2.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 0 - 25 °C

3.1: copper(l) chloride / ethanol / 14 h / 70 °C

4.1: N-ethyl-N,N-diisopropylamine; dmap / 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran / 16 h / 30 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

5.2: 1 h / -78 °C

6.1: boron tribromide / dichloromethane / -78 - 25 °C

6.2: 4 h / 25 °C

7.1: nitric acid; sulfuric acid / 2 h / -10 °C

7.2: 25 °C

7.3: Chiral PAK AD column / Resolution of racemate

8.1: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 40 °C

With hydrogenchloride; dmap; n-butyllithium; sulfuric acid; palladium 10% on activated carbon; hydrogen; nitric acid; boron tribromide; N-ethyl-N,N-diisopropylamine; copper(l) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; dichloromethane; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran;

Reference yield:

: 1402742-11-3
C₁₅H₁₃FO₂

: 1616109-94-4
C₁₉H₂₆FN₃O₅S

Guidance literature:: Multi-step reaction with 9 steps

1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 16 h / 25 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 3 h / -78 °C

3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 0 - 25 °C

4.1: copper(l) chloride / ethanol / 14 h / 70 °C

5.1: N-ethyl-N,N-diisopropylamine; dmap / 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran / 16 h / 30 °C

6.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

6.2: 1 h / -78 °C

7.1: boron tribromide / dichloromethane / -78 - 25 °C

7.2: 4 h / 25 °C

8.1: nitric acid; sulfuric acid / 2 h / -10 °C

8.2: 25 °C

8.3: Chiral PAK AD column / Resolution of racemate

9.1: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 40 °C

With hydrogenchloride; dmap; titanium(IV) tetraethanolate; n-butyllithium; sulfuric acid; palladium 10% on activated carbon; hydrogen; nitric acid; boron tribromide; N-ethyl-N,N-diisopropylamine; copper(l) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; dichloromethane; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran;