(Z)-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)hex-2-enoic acid 8-phenylmenthyl ester

Base Information

Chemical Name:(Z)-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)hex-2-enoic acid 8-phenylmenthyl ester
CAS No.:1059067-69-4
Molecular Formula:C₃₆H₅₃NO₅Si
Molecular Weight:607.906
Hs Code.:

Synonyms:(Z)-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)hex-2-enoic acid 8-phenylmenthyl ester

Suppliers and Price of (Z)-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)hex-2-enoic acid 8-phenylmenthyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)hex-2-enoic acid 8-phenylmenthyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)hex-2-enoic acid 8-phenylmenthyl ester

There total 1 articles about (Z)-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)hex-2-enoic acid 8-phenylmenthyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 917603-60-2
benzyloxycarbonylamino(diethoxyphosphoryl)acetic acid (-)-8-phenylmenthyl ester

: 87184-81-4
4-(tert-butyldimethylsilanyloxy)butanal

: 1059067-69-4
(Z)-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)hex-2-enoic acid 8-phenylmenthyl ester

Guidance literature:: benzyloxycarbonylamino(diethoxyphosphoryl)acetic acid (-)-8-phenylmenthyl ester; With N,N,N',N'-tetramethylguanidine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

4-(tert-butyldimethylsilanyloxy)butanal; In dichloromethane; for 24h;
DOI:10.1021/ol801709c

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 1059067-69-4
(Z)-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)hex-2-enoic acid 8-phenylmenthyl ester

: 1059067-67-2
(2S,3E)-2-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)-2-benzyloxymethylhex-3-enoic acid 8-phenylmenthyl ester

Guidance literature:: (Z)-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)hex-2-enoic acid 8-phenylmenthyl ester; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

Benzyloxymethyl chloride; In tetrahydrofuran; hexane; at -78 ℃; for 7h; Inert atmosphere;
DOI:10.1021/ol801709c