2,2′,2″,2?‐[(carbonylbis(benzene‐4,1,3‐triyl))tetrakis(oxy)]tetraacetic acid

Base Information

Chemical Name:2,2′,2″,2?‐[(carbonylbis(benzene‐4,1,3‐triyl))tetrakis(oxy)]tetraacetic acid
CAS No.:1207268-56-1
Molecular Formula:C₂₁H₁₈O₁₃
Molecular Weight:478.366
Hs Code.:

Synonyms:2,2′,2″,2?‐[(carbonylbis(benzene‐4,1,3‐triyl))tetrakis(oxy)]tetraacetic acid

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Chemical Property of 2,2′,2″,2?‐[(carbonylbis(benzene‐4,1,3‐triyl))tetrakis(oxy)]tetraacetic acid

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Technology Process of 2,2′,2″,2?‐[(carbonylbis(benzene‐4,1,3‐triyl))tetrakis(oxy)]tetraacetic acid

There total 2 articles about 2,2′,2″,2?‐[(carbonylbis(benzene‐4,1,3‐triyl))tetrakis(oxy)]tetraacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: tetramethyl 2,2′,2″,2?‐[(carbonylbis(benzene‐4,1,3‐triyl))tetrakis(oxy)]tetraacetate

: 1207268-56-1
2,2′,2″,2?‐[(carbonylbis(benzene‐4,1,3‐triyl))tetrakis(oxy)]tetraacetic acid

Guidance literature:: With sodium hydroxide; In methanol; dichloromethane; at 20 ℃; for 24h;
DOI:10.1002/chir.23142

Reference yield:

: 131-55-5
2,2',4,4'-tetrahydroxybenzophenone

: 1207268-56-1
2,2′,2″,2?‐[(carbonylbis(benzene‐4,1,3‐triyl))tetrakis(oxy)]tetraacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 24 h / Reflux

2: sodium hydroxide / methanol; dichloromethane / 24 h / 20 °C

With potassium carbonate; sodium hydroxide; In methanol; dichloromethane; acetone; 1: |Williamson Ether Synthesis;
DOI:10.1002/chir.23142

Reference yield: 87.0%

: 1207268-56-1
2,2′,2″,2?‐[(carbonylbis(benzene‐4,1,3‐triyl))tetrakis(oxy)]tetraacetic acid

: 20989-17-7
(2S)-2-phenylglycinol

: 2,2',2'',2'''-{carbonylbis[benzene-4,1,3-triyltetrakis(oxy)]}tetrakis{N-[(S)-2-hydroxy-1-phenylethyl]acetamide}

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1002/chir.23297