C₁₆H₁₃ClO₃S

Base Information

• Chemical Name: C₁₆H₁₃ClO₃S
• CAS No.: 57077-20-0
• Molecular Formula: C₁₆H₁₃ClO₃S
• Molecular Weight: 320.796
• Mol file: 57077-20-0.mol

Synonyms:C₁₆H₁₃ClO₃S

Chemical Property of C₁₆H₁₃ClO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₆H₁₃ClO₃S

There total 1 articles about C₁₆H₁₃ClO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

4-(methanesulfonyl)acetophenone (10297-73-1) + 4-chlorobenzaldehyde (104-88-1) → C16H13ClO3S (57077-20-0)

Guidance literature:

With barium hydroxide octahydrate; In ethanol; at 30 ℃; for 24h;

DOI:10.1016/j.ejmech.2010.10.005

Reference yield: 97.0%

C16H13ClO3S (57077-20-0) + 4-fluorophenyhydrazine hydrochloride (823-85-8) → 1-(4-fluorophenyl)-5-(4-chlorophenyl)-3-(4-(methylsulfonyl)phenyl)-4,5-dihydro-1H-pyrazole

Guidance literature:

In acetic acid; for 8h; Reflux;

DOI:10.3390/molecules20022668

Reference yield: 83.0%

C16H13ClO3S (57077-20-0) + 4-bromophenylhydrazine hydrochloride (622-88-8,41931-18-4) → 1-(4-bromophenyl)-5-(4-chlorophenyl)-3-(4-(methylsulfonyl)phenyl)-4,5-dihydro-1H-pyrazole

Guidance literature:

In acetic acid; for 8h; Reflux;

DOI:10.3390/molecules20022668

upstream raw materials:

4-(methanesulfonyl)acetophenone

4-chlorobenzaldehyde

Downstream raw materials:

C₁₈H₁₇ClN₂O₃S

C₁₇H₁₆ClN₃O₂S₂