Cyclohexylmethyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

Base Information

Chemical Name:Cyclohexylmethyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside
CAS No.:133339-65-8
Molecular Formula:C₂₂H₃₂Cl₃NO₁₀
Molecular Weight:576.856
Hs Code.:

Synonyms:Cyclohexylmethyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

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Chemical Property of Cyclohexylmethyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

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Technology Process of Cyclohexylmethyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

There total 3 articles about Cyclohexylmethyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 122210-05-3
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranose

: 88773-80-2
cyclohexylmethyl trimethylsilyl ether

: 133339-65-8
Cyclohexylmethyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

Guidance literature:: With tin(II) trifluoromethanesulfonate; In dichloromethane; for 6h; Ambient temperature;

Reference yield: 87.0%

: 67124-60-1
3,4,6-Tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranosyl bromide

: 100-49-2
cyclohexylmethyl alcohol

: 133339-65-8
Cyclohexylmethyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

Guidance literature:: With trityl chloride; zinc(II) chloride; In dichloromethane; for 13h; Ambient temperature;
DOI:10.1248/cpb.38.3280

Reference yield:

: 122210-01-9
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 133339-65-8
Cyclohexylmethyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 25percent HBr-AcOH / 2 h / Ambient temperature

2: 87 percent / ZnCl₂, TrCl / CH₂Cl₂ / 13 h / Ambient temperature

With hydrogen bromide; trityl chloride; acetic acid; zinc(II) chloride; In dichloromethane;
DOI:10.1248/cpb.38.3280