2-bromo-5-[[[3-[[t-butyl(dimethyl)silyl]oxy]propyl]thio](2,3,6-trifluorophenyl)methyl]-4-methylpyridine

Base Information

Chemical Name:2-bromo-5-[[[3-[[t-butyl(dimethyl)silyl]oxy]propyl]thio](2,3,6-trifluorophenyl)methyl]-4-methylpyridine
CAS No.:1132842-66-0
Molecular Formula:C₂₂H₂₉BrF₃NOSSi
Molecular Weight:520.529
Hs Code.:

Synonyms:2-bromo-5-[[[3-[[t-butyl(dimethyl)silyl]oxy]propyl]thio](2,3,6-trifluorophenyl)methyl]-4-methylpyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-5-[[[3-[[t-butyl(dimethyl)silyl]oxy]propyl]thio](2,3,6-trifluorophenyl)methyl]-4-methylpyridine

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Technology Process of 2-bromo-5-[[[3-[[t-butyl(dimethyl)silyl]oxy]propyl]thio](2,3,6-trifluorophenyl)methyl]-4-methylpyridine

There total 1 articles about 2-bromo-5-[[[3-[[t-butyl(dimethyl)silyl]oxy]propyl]thio](2,3,6-trifluorophenyl)methyl]-4-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1132842-58-0
(6-bromo-4-methylpyridin-3-yl)(2,3,6-trifluorophenyl)methanethiol

: 89031-84-5
3-(tert-butyldimethylsilyloxy)propyl bromide

: 1132842-66-0
2-bromo-5-[[[3-[[t-butyl(dimethyl)silyl]oxy]propyl]thio](2,3,6-trifluorophenyl)methyl]-4-methylpyridine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃;

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 1132842-66-0
2-bromo-5-[[[3-[[t-butyl(dimethyl)silyl]oxy]propyl]thio](2,3,6-trifluorophenyl)methyl]-4-methylpyridine

: C₂₃H₃₀F₃NO₃SSi

Guidance literature:: 2-bromo-5-[[[3-[[t-butyl(dimethyl)silyl]oxy]propyl]thio](2,3,6-trifluorophenyl)methyl]-4-methylpyridine; With n-butyllithium; In hexane; toluene; at -78 - -40 ℃; Inert atmosphere;

carbon dioxide; In hexane; toluene; at -78 - 20 ℃; for 0.333333h;

With ammonium chloride; In hexane; water; toluene;