2-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-ylmethyl)-cyclohexanone

Base Information

• Chemical Name: 2-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-ylmethyl)-cyclohexanone
• CAS No.: 474640-40-9
• Molecular Formula: C₁₇H₂₃NO₄S
• Molecular Weight: 337.44

Synonyms:2-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-ylmethyl)-cyclohexanone

Chemical Property of 2-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-ylmethyl)-cyclohexanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-ylmethyl)-cyclohexanone

There total 3 articles about 2-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-ylmethyl)-cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

dithiocarbonic acid O-ethyl ester S-[2-[methanesulfonyl-(4-methoxy-phenyl)-amino]-1-(2-oxo-cyclohexylmethyl)-ethyl] ester (474640-37-4) → 2-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-ylmethyl)-cyclohexanone (474640-40-9)

Guidance literature:

With dilauryl peroxide; In 1,2-dichloro-ethane; Heating;

DOI:10.1039/b204371h

Reference yield:

N-(4-methoxyphenyl)-N-(prop-2-en-1-yl)methanesulfonamide (23004-83-3) → 2-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-ylmethyl)-cyclohexanone (474640-40-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

2: 66 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

With dilauryl peroxide; In 1,2-dichloro-ethane;

DOI:10.1039/b204371h

Reference yield:

ethyl [(2-oxocyclohexyl)sulfanyl]methanethioate (82721-86-6) → 2-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-ylmethyl)-cyclohexanone (474640-40-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

2: 66 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

With dilauryl peroxide; In 1,2-dichloro-ethane;

DOI:10.1039/b204371h

upstream raw materials:

dithiocarbonic acid O-ethyl ester S-[2-[methanesulfonyl-(4-methoxy-phenyl)-amino]-1-(2-oxo-cyclohexylmethyl)-ethyl] ester

N-(4-methoxyphenyl)-N-(prop-2-en-1-yl)methanesulfonamide

ethyl [(2-oxocyclohexyl)sulfanyl]methanethioate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 474640-40-9 2-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-ylmethyl)-cyclohexanone

Send

Send

Metric Ton KG G Pound L ML

Send

Send