11-bromo-8α,9β-bis(benzoyloxy)-8,9,10,11-tetrahydrobenzofluoranthene

Base Information

Chemical Name:11-bromo-8α,9β-bis(benzoyloxy)-8,9,10,11-tetrahydrobenzofluoranthene
CAS No.:77061-21-3
Molecular Formula:C₃₄H₂₃BrO₄
Molecular Weight:575.458
Hs Code.:

11-bromo-8α,9β-bis(benzoyloxy)-8,9,10,11-tetrahydrobenzo<k>fluoranthene

Synonyms:11-bromo-8α,9β-bis(benzoyloxy)-8,9,10,11-tetrahydrobenzofluoranthene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11-bromo-8α,9β-bis(benzoyloxy)-8,9,10,11-tetrahydrobenzofluoranthene

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Technology Process of 11-bromo-8α,9β-bis(benzoyloxy)-8,9,10,11-tetrahydrobenzofluoranthene

There total 1 articles about 11-bromo-8α,9β-bis(benzoyloxy)-8,9,10,11-tetrahydrobenzofluoranthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 77061-20-2
trans-8,9-bis(benzoyloxy)-8,9,10,11-tetrahydrobenzofluoranthene

: 77061-21-3
11-bromo-8α,9β-bis(benzoyloxy)-8,9,10,11-tetrahydrobenzofluoranthene

Guidance literature:: With N-Bromosuccinimide; azobisisobutyronitrile; In tetrachloromethane; for 2h; Heating;
DOI:10.1021/jo00325a028

Reference yield: 60.0%

: 77061-21-3
11-bromo-8α,9β-bis(benzoyloxy)-8,9,10,11-tetrahydrobenzofluoranthene

: 77061-22-4
trans-8,9-bis(benzoyloxy)-8,9-dihydrobenzofluoranthene

Guidance literature:: With DBN; In tetrahydrofuran; at 0 ℃; for 3h;
DOI:10.1021/jo00325a028

Reference yield:

: 77061-21-3
11-bromo-8α,9β-bis(benzoyloxy)-8,9,10,11-tetrahydrobenzofluoranthene

: 76479-15-7,100310-95-0
trans-8,9-dihydro-8,9-dihydroxybenzofluoranthene

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / 1,5-diazabicyclo<4.3.0>non-5-ene / tetrahydrofuran / 3 h / 0 °C

2: 38 percent / sodium methoxide / tetrahydrofuran; methanol / 0.5 h / Ambient temperature

With DBN; sodium methylate; In tetrahydrofuran; methanol;
DOI:10.1021/jo00325a028