C₁₈H₂₆FNO₅

Base Information

Chemical Name:C₁₈H₂₆FNO₅
CAS No.:1354973-70-8
Molecular Formula:C₁₈H₂₆FNO₅
Molecular Weight:355.407
Hs Code.:

C<sub>18</sub>H<sub>26</sub>FNO<sub>5</sub>

Synonyms:C₁₈H₂₆FNO₅

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Chemical Property of C₁₈H₂₆FNO₅

Chemical Property:

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Technology Process of C₁₈H₂₆FNO₅

There total 12 articles about C₁₈H₂₆FNO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 1354973-69-5
C₂₂H₃₅NO₅

: 1354973-70-8
C₁₈H₂₆FNO₅

Guidance literature:: With pyridine hydrogenfluoride; bis-[(trifluoroacetoxy)iodo]benzene; In dichloromethane; at 20 ℃; for 0.333333h;

Reference yield:

: 38473-89-1
3-bromo-4-(tert-butyl)benzoic acid

: 1354973-70-8
C₁₈H₂₆FNO₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: borane-THF / tetrahydrofuran / 13 h / 0 - 20 °C

1.2: 22 h / 20 °C

2.1: potassium dihydrogenphosphate; trifluoroacetyl peroxide / dichloromethane / 1 h / 0 °C

2.2: 0.17 h / 20 °C

3.1: dmap; 1H-imidazole / dichloromethane / 20 °C

4.1: n-butyllithium / hexane; tetrahydrofuran / 0.53 h / -78 °C

4.2: 0.5 h / -78 °C

5.1: water; sodium tetrahydroborate / ethanol / 0.13 h / 0 °C

6.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 0.3 h / 20 °C

7.1: (2S,4S,5R)-1-(anthracen-9-ylmethyl)-5-ethenyl-2-[(R)-(prop-2-en-1-yloxy)(quinolin-4-yl)methyl]-1-azabicyclo[2.2.2]octan-1-ium bromide; cesiumhydroxide monohydrate / dichloromethane / 36 h / -60 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.45 h / 0 °C

9.1: hydrogenchloride / water; tetrahydrofuran / 0.67 h / Inert atmosphere

10.1: sodium hydrogencarbonate / 1,4-dioxane; water / 2.25 h

11.1: bis-[(trifluoroacetoxy)iodo]benzene; pyridine hydrogenfluoride / dichloromethane / 0.33 h / 20 °C

With 1H-imidazole; hydrogenchloride; dmap; sodium tetrahydroborate; potassium dihydrogenphosphate; n-butyllithium; borane-THF; cesiumhydroxide monohydrate; trifluoroacetyl peroxide; tetrabutyl ammonium fluoride; water; iodine; sodium hydrogencarbonate; pyridine hydrogenfluoride; triphenylphosphine; bis-[(trifluoroacetoxy)iodo]benzene; (2S,4S,5R)-1-(anthracen-9-ylmethyl)-5-ethenyl-2-[(R)-(prop-2-en-1-yloxy)(quinolin-4-yl)methyl]-1-azabicyclo[2.2.2]octan-1-ium bromide; In tetrahydrofuran; 1,4-dioxane; ethanol; hexane; dichloromethane; water;

Reference yield:

: 129167-73-3
3-bromo-4-(tert-butyl)benzaldehyde

: 1354973-70-8
C₁₈H₂₆FNO₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium dihydrogenphosphate; trifluoroacetyl peroxide / dichloromethane / 1 h / 0 °C

1.2: 0.17 h / 20 °C

2.1: dmap; 1H-imidazole / dichloromethane / 20 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.53 h / -78 °C

3.2: 0.5 h / -78 °C

4.1: water; sodium tetrahydroborate / ethanol / 0.13 h / 0 °C

5.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 0.3 h / 20 °C

6.1: (2S,4S,5R)-1-(anthracen-9-ylmethyl)-5-ethenyl-2-[(R)-(prop-2-en-1-yloxy)(quinolin-4-yl)methyl]-1-azabicyclo[2.2.2]octan-1-ium bromide; cesiumhydroxide monohydrate / dichloromethane / 36 h / -60 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.45 h / 0 °C

8.1: hydrogenchloride / water; tetrahydrofuran / 0.67 h / Inert atmosphere

9.1: sodium hydrogencarbonate / 1,4-dioxane; water / 2.25 h

10.1: bis-[(trifluoroacetoxy)iodo]benzene; pyridine hydrogenfluoride / dichloromethane / 0.33 h / 20 °C

With 1H-imidazole; hydrogenchloride; dmap; sodium tetrahydroborate; potassium dihydrogenphosphate; n-butyllithium; cesiumhydroxide monohydrate; trifluoroacetyl peroxide; tetrabutyl ammonium fluoride; water; iodine; sodium hydrogencarbonate; pyridine hydrogenfluoride; triphenylphosphine; bis-[(trifluoroacetoxy)iodo]benzene; (2S,4S,5R)-1-(anthracen-9-ylmethyl)-5-ethenyl-2-[(R)-(prop-2-en-1-yloxy)(quinolin-4-yl)methyl]-1-azabicyclo[2.2.2]octan-1-ium bromide; In tetrahydrofuran; 1,4-dioxane; ethanol; hexane; dichloromethane; water;