N-(4-methoxybenzyl)-N-(5-(4-methoxybenzyloxy)pentyl)-4-methylbenzenesulfonamide

Base Information

• Chemical Name: N-(4-methoxybenzyl)-N-(5-(4-methoxybenzyloxy)pentyl)-4-methylbenzenesulfonamide
• CAS No.: 1402581-07-0
• Molecular Formula: C₂₈H₃₅NO₅S
• Molecular Weight: 497.656

Synonyms:N-(4-methoxybenzyl)-N-(5-(4-methoxybenzyloxy)pentyl)-4-methylbenzenesulfonamide

Chemical Property of N-(4-methoxybenzyl)-N-(5-(4-methoxybenzyloxy)pentyl)-4-methylbenzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(4-methoxybenzyl)-N-(5-(4-methoxybenzyloxy)pentyl)-4-methylbenzenesulfonamide

There total 2 articles about N-(4-methoxybenzyl)-N-(5-(4-methoxybenzyloxy)pentyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

N-(5-hydroxypentyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide (1402581-09-2) + p-methoxybenzyl chloride (824-94-2) → N-(4-methoxybenzyl)-N-(5-(4-methoxybenzyloxy)pentyl)-4-methylbenzenesulfonamide (1402581-07-0)

Guidance literature:

N-(5-hydroxypentyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.333333h;

p-methoxybenzyl chloride; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; mineral oil; at 20 ℃;

DOI:10.1021/jo301787v

Reference yield:

p-methoxybenzyl chloride (824-94-2) → N-(4-methoxybenzyl)-N-(5-(4-methoxybenzyloxy)pentyl)-4-methylbenzenesulfonamide (1402581-07-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

1.2: 20 °C

2.1: silver hexafluoroantimonate; water / dichloromethane / 5 h / 40 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

3.2: 20 °C

With silver hexafluoroantimonate; water; sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;

DOI:10.1021/jo301787v

Reference yield: 80.0%

N-(4-methoxybenzyl)-N-(5-(4-methoxybenzyloxy)pentyl)-4-methylbenzenesulfonamide (1402581-07-0) → N-(5-hydroxypentyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide (1402581-09-2) + N-(5-hydroxy-pentyl)-4-methyl-benzenesulfonamide (16780-44-2)

Guidance literature:

With silver hexafluoroantimonate; 1,2,3-trimethoxybenzene; In dichloromethane; at 40 ℃; for 16h;

DOI:10.1021/jo301787v

upstream raw materials:

N-(5-hydroxypentyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

p-methoxybenzyl chloride

Downstream raw materials:

N-(5-hydroxypentyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

N-(5-hydroxy-pentyl)-4-methyl-benzenesulfonamide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1402581-07-0 N-(4-methoxybenzyl)-N-(5-(4-methoxybenzyloxy)pentyl)-4-methylbenzenesulfonamide

Send

Send

Metric Ton KG G Pound L ML

Send

Send