C₁₂H₁₅NO₃

Base Information

• Chemical Name: C₁₂H₁₅NO₃
• CAS No.: 1023294-64-5
• Molecular Formula: C₁₂H₁₅NO₃
• Molecular Weight: 221.256
• Mol file: 1023294-64-5.mol

Synonyms:C₁₂H₁₅NO₃

Chemical Property of C₁₂H₁₅NO₃

Chemical Property:

Purity/Quality:

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Technology Process of C₁₂H₁₅NO₃

There total 1 articles about C₁₂H₁₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2,4-dimethoxyphenyl)but-3-en-1-one (15852-68-3) → C12H15NO3 (1023294-64-5)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; at 20 ℃;

DOI:10.1021/ol8002173

Reference yield: 73.0%

C12H15NO3 (1023294-64-5) + tert-butyl-4-bromobenzoate (59247-47-1) → C23H27NO5 (1023294-76-9)

Guidance literature:

With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; In toluene; at 105 ℃; for 3h; Inert atmosphere;

DOI:10.1021/ol8002173

upstream raw materials:

1-(2,4-dimethoxyphenyl)but-3-en-1-one

Downstream raw materials:

C₂₃H₂₇NO₅