(S)-2-Amino-N-(3-hydrazinocarbonyl-2-oxo-2H-chromen-6-yl)-3-phenyl-propionamide; hydrochloride

Base Information

Chemical Name:(S)-2-Amino-N-(3-hydrazinocarbonyl-2-oxo-2H-chromen-6-yl)-3-phenyl-propionamide; hydrochloride
CAS No.:80613-72-5
Molecular Formula:C₁₉H₁₈N₄O₄*ClH
Molecular Weight:402.837
Hs Code.:

Synonyms:(S)-2-Amino-N-(3-hydrazinocarbonyl-2-oxo-2H-chromen-6-yl)-3-phenyl-propionamide; hydrochloride

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Chemical Property of (S)-2-Amino-N-(3-hydrazinocarbonyl-2-oxo-2H-chromen-6-yl)-3-phenyl-propionamide; hydrochloride

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Technology Process of (S)-2-Amino-N-(3-hydrazinocarbonyl-2-oxo-2H-chromen-6-yl)-3-phenyl-propionamide; hydrochloride

There total 3 articles about (S)-2-Amino-N-(3-hydrazinocarbonyl-2-oxo-2H-chromen-6-yl)-3-phenyl-propionamide; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 80613-62-3
6-(N-Phthalyl-L-Phe)aminocoumarin-3-carboxylic acid methyl ester

: 80613-72-5
(S)-2-Amino-N-(3-hydrazinocarbonyl-2-oxo-2H-chromen-6-yl)-3-phenyl-propionamide; hydrochloride

Guidance literature:: With hydrogenchloride; hydrazine hydrate; In tetralin; ethanol; Heating;
DOI:10.1002/jhet.5570180627

Reference yield:

: 80613-57-6
6-aminocoumarin-3-carboxylic acid methyl ester

: 80613-72-5
(S)-2-Amino-N-(3-hydrazinocarbonyl-2-oxo-2H-chromen-6-yl)-3-phenyl-propionamide; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / triethylamine / dioxane / 1) room temperature, 2) 3 h, reflux

2: 79 percent / 1)0.5 M hydrazine hydrate, 2) HCl / 1,2,3,4-tetrahydro-naphthalene; ethanol / Heating

With hydrogenchloride; hydrazine hydrate; triethylamine; In 1,4-dioxane; tetralin; ethanol;
DOI:10.1002/jhet.5570180627

Reference yield:

: 32150-91-7
phthaloyl-L-phenylalanyl chloride

: 80613-72-5
(S)-2-Amino-N-(3-hydrazinocarbonyl-2-oxo-2H-chromen-6-yl)-3-phenyl-propionamide; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / triethylamine / dioxane / 1) room temperature, 2) 3 h, reflux

2: 79 percent / 1)0.5 M hydrazine hydrate, 2) HCl / 1,2,3,4-tetrahydro-naphthalene; ethanol / Heating

With hydrogenchloride; hydrazine hydrate; triethylamine; In 1,4-dioxane; tetralin; ethanol;
DOI:10.1002/jhet.5570180627