tert-butyl 5-chloro-4-(3-chloro-4-(trifluoromethoxy)-phenoxy)-2-fluorobenzoate

Base Information

Chemical Name:tert-butyl 5-chloro-4-(3-chloro-4-(trifluoromethoxy)-phenoxy)-2-fluorobenzoate
CAS No.:1354962-92-7
Molecular Formula:C₁₈H₁₄Cl₂F₄O₄
Molecular Weight:441.206
Hs Code.:

Synonyms:tert-butyl 5-chloro-4-(3-chloro-4-(trifluoromethoxy)-phenoxy)-2-fluorobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 5-chloro-4-(3-chloro-4-(trifluoromethoxy)-phenoxy)-2-fluorobenzoate

Chemical Property:

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Technology Process of tert-butyl 5-chloro-4-(3-chloro-4-(trifluoromethoxy)-phenoxy)-2-fluorobenzoate

There total 2 articles about tert-butyl 5-chloro-4-(3-chloro-4-(trifluoromethoxy)-phenoxy)-2-fluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1000339-94-5
3-chloro-4-(trifluoromethoxy)phenol

: 1354961-13-9
tert-butyl-5-chloro-2,4-di-fluorobenzoate

: 1354962-92-7
tert-butyl 5-chloro-4-(3-chloro-4-(trifluoromethoxy)-phenoxy)-2-fluorobenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 19h;

Reference yield:

: 5-chloro-2,4-difluorobenzoic acid

: 1354962-92-7
tert-butyl 5-chloro-4-(3-chloro-4-(trifluoromethoxy)-phenoxy)-2-fluorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / tert-butyl alcohol / 16 h / 50 °C

2: potassium carbonate / dimethyl sulfoxide / 18 h / 20 °C

With dmap; potassium carbonate; In dimethyl sulfoxide; tert-butyl alcohol;

Reference yield:

: 1354962-92-7
tert-butyl 5-chloro-4-(3-chloro-4-(trifluoromethoxy)-phenoxy)-2-fluorobenzoate

: 1354955-46-6
5-chloro-4-[-3-chloro-4-(trifluoromethoxy)phenoxy]-2-fluoro-N-(methylsulfonyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 54 h / 20 °C

2: N-ethyl-N,N-diisopropylamine; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide / ethyl acetate; tetrahydrofuran / 18 h / Reflux

With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; ethyl acetate;