N-demethylthevinone

Base Information

Chemical Name:N-demethylthevinone
CAS No.:16553-22-3
Molecular Formula:C₂₂H₂₅NO₄
Molecular Weight:367.445
Hs Code.:

Synonyms:N-demethylthevinone

Suppliers and Price of N-demethylthevinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-demethylthevinone

Chemical Property:

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Technology Process of N-demethylthevinone

There total 1 articles about N-demethylthevinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1234788-69-2
thevinone-N-oxide hydrochloride

: 16553-22-3
N-demethylthevinone

: 15358-22-2
thevinone

Guidance literature:: With iron; In isopropyl alcohol; at 60 ℃; Inert atmosphere;
DOI:10.1021/jo1008492

Reference yield: 76.0%

: 16553-22-3
N-demethylthevinone

: 103-63-9
1-phenyl-2-bromoethane

: 16553-33-6
1-(4,5α-epoxy-3,6-dimethoxy-17-phenethyl-6α,14α-etheno-morphinan-7α-yl)-ethanone

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 90 ℃; for 20h;
DOI:10.1016/S0968-0896(96)00257-X

Reference yield:

: 16553-22-3
N-demethylthevinone

: C₃₀H₃₅NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / NaHCO₃ / dimethylformamide / 20 h / 90 °C

2: 68 percent / toluene; diethyl ether / 1 h / Heating

3: KOH / bis-(2-hydroxy-ethyl) ether / 1.5 h / 210 - 220 °C

With potassium hydroxide; sodium hydrogencarbonate; In diethyl ether; N,N-dimethyl-formamide; toluene; diethylene glycol;
DOI:10.1016/S0968-0896(96)00257-X