As(C₁₀H₄S₂(NC₆H₄OCH₃)2)⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₁₀H₄S₂(NC₆H₄OCH₃)2)As]O₃SCF₃

Base Information

Chemical Name:As(C₁₀H₄S₂(NC₆H₄OCH₃)2)⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₁₀H₄S₂(NC₆H₄OCH₃)2)As]O₃SCF₃
CAS No.:1349037-52-0
Molecular Formula:CF₃O₃S*C₂₄H₁₈AsN₂O₂S₂
Molecular Weight:654.543
Hs Code.:

As(C<sub>10</sub>H<sub>4</sub>S<sub>2</sub>(NC<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)2)<sup>(1+)</sup>*O<sub>3</sub>SCF<sub>3</sub><sup>(1-)</sup>=[(C<sub>10</sub>H<sub>4</sub>S<sub>2</sub>(NC<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)2)As]O<sub>3</sub>SCF<sub>3</sub>

Synonyms:As(C₁₀H₄S₂(NC₆H₄OCH₃)2)⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₁₀H₄S₂(NC₆H₄OCH₃)2)As]O₃SCF₃

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Chemical Property of As(C₁₀H₄S₂(NC₆H₄OCH₃)2)⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₁₀H₄S₂(NC₆H₄OCH₃)2)As]O₃SCF₃

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Technology Process of As(C₁₀H₄S₂(NC₆H₄OCH₃)2)⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₁₀H₄S₂(NC₆H₄OCH₃)2)As]O₃SCF₃

There total 2 articles about As(C₁₀H₄S₂(NC₆H₄OCH₃)2)⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₁₀H₄S₂(NC₆H₄OCH₃)2)As]O₃SCF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1349037-47-3
C₂₄H₁₈AsClN₂O₂S₂

: 1349037-52-0
As(C₁₀H₄S₂(NC₆H₄OCH₃)2)⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₁₀H₄S₂(NC₆H₄OCH₃)2)As]O₃SCF₃

Guidance literature:: In dichloromethane; at 20 ℃; for 0.75h; Inert atmosphere;
DOI:10.1021/ic201983n

Reference yield:

: 1349037-45-1
C₁₀H₄S₂(NHC₆H₄OCH₃)2

: 1349037-52-0
As(C₁₀H₄S₂(NC₆H₄OCH₃)2)⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₁₀H₄S₂(NC₆H₄OCH₃)2)As]O₃SCF₃

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine; arsenic trichloride / tetrahydrofuran / 96 h / 20 °C / Inert atmosphere

2: dichloromethane / 0.75 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; arsenic trichloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ic201983n

Reference yield: 92.0%

: 14221-02-4
tetrakis(triphenylphosphine)platinum

: 1349037-52-0
As(C₁₀H₄S₂(NC₆H₄OCH₃)2)⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₁₀H₄S₂(NC₆H₄OCH₃)2)As]O₃SCF₃

: Pt(As(C₁₀H₄S₂(NC₆H₄OCH₃)2))(P(C₆H₅)3)2⁽¹⁺⁾*O₃SCF₃^(1-)=[Pt(As(C₁₀H₄S₂(NC₆H₄OCH₃)2))(P(C₆H₅)3)2]O₃SCF₃

Guidance literature:: In dichloromethane; byproducts: P(C6H5)3; under N2, Schlenk technique; soln. of Pt complex in CH2Cl2 added to soln. of As compd. in CH2Cl2, mixt. stirred at room temp. for 10 min; evapn. under vac., oily residue triturated with Et2O for 10 min, solid sepd. by decantation, dried under vac.;
DOI:10.1021/ic201983n