<((p. dihydroxy-2,3 propoxy) benzoyl methyl)-4 piperazinyl-1>-2 ethoxycarbonyl-6 ethyl-8 oxo-5 dihydro-5,8 pyrido <2,3-d> pyrimidine

Base Information

Chemical Name:<((p. dihydroxy-2,3 propoxy) benzoyl methyl)-4 piperazinyl-1>-2 ethoxycarbonyl-6 ethyl-8 oxo-5 dihydro-5,8 pyrido <2,3-d> pyrimidine
CAS No.:68689-68-9
Molecular Formula:C₂₇H₃₃N₅O₇
Molecular Weight:539.588
Hs Code.:

Synonyms:<((p. dihydroxy-2,3 propoxy) benzoyl methyl)-4 piperazinyl-1>-2 ethoxycarbonyl-6 ethyl-8 oxo-5 dihydro-5,8 pyrido <2,3-d> pyrimidine

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Chemical Property of <((p. dihydroxy-2,3 propoxy) benzoyl methyl)-4 piperazinyl-1>-2 ethoxycarbonyl-6 ethyl-8 oxo-5 dihydro-5,8 pyrido <2,3-d> pyrimidine

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Technology Process of <((p. dihydroxy-2,3 propoxy) benzoyl methyl)-4 piperazinyl-1>-2 ethoxycarbonyl-6 ethyl-8 oxo-5 dihydro-5,8 pyrido <2,3-d> pyrimidine

There total 3 articles about <((p. dihydroxy-2,3 propoxy) benzoyl methyl)-4 piperazinyl-1>-2 ethoxycarbonyl-6 ethyl-8 oxo-5 dihydro-5,8 pyrido <2,3-d> pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 69886-87-9
chloro-1 propane diol-1,3

: ethoxycarbonyl-6 ethyl-8 <(hydroxy-4 benzoylmethyl)-4 piperazinyl-1>-2 oxo-5 dihydro-5,8 pyrido <2,3-d> pyrimidine

: 68689-68-9
<((p. dihydroxy-2,3 propoxy) benzoyl methyl)-4 piperazinyl-1>-2 ethoxycarbonyl-6 ethyl-8 oxo-5 dihydro-5,8 pyrido <2,3-d> pyrimidine

Guidance literature:: With sodium ethanolate; In ethanol; for 6h; Heating;

Reference yield:

: 2491-37-4
2-bromo-1-(3-hydroxyphenyl)ethanone

: 68689-68-9
<((p. dihydroxy-2,3 propoxy) benzoyl methyl)-4 piperazinyl-1>-2 ethoxycarbonyl-6 ethyl-8 oxo-5 dihydro-5,8 pyrido <2,3-d> pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / triethylamine / CHCl₃ / 2 h / Heating

2: 48 percent / ethylate de sodium / ethanol / 6 h / Heating

With sodium ethanolate; triethylamine; In ethanol; chloroform;

Reference yield:

: 51940-43-3
ethyl 5,8-dihydro-8-ethyl-2-(1-piperazinyl)-5-oxopyrido[2,3-d]pyrimidine-6-carboxylate

: 68689-68-9
<((p. dihydroxy-2,3 propoxy) benzoyl methyl)-4 piperazinyl-1>-2 ethoxycarbonyl-6 ethyl-8 oxo-5 dihydro-5,8 pyrido <2,3-d> pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / triethylamine / CHCl₃ / 2 h / Heating

2: 48 percent / ethylate de sodium / ethanol / 6 h / Heating

With sodium ethanolate; triethylamine; In ethanol; chloroform;