Technology Process of 2-formyl-5-methoxyphenyl but-3-enoate
There total 1 articles about 2-formyl-5-methoxyphenyl but-3-enoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
but-3-enoic acid;
With
dicyclohexyl-carbodiimide;
In
dichloromethane;
for 1h;
2-Hydroxy-4-methoxybenzaldehyde;
With
dmap;
In
dichloromethane;
for 2h;
DOI:10.1021/ol201983u
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium tert-butylate / tetrahydrofuran
2: sodium acetate; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 80 °C
With
potassium tert-butylate; sodium acetate; palladium diacetate; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
2: Heck reaction;
DOI:10.1021/ol201983u
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium tert-butylate / tetrahydrofuran
2: sodium acetate; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 80 °C
With
potassium tert-butylate; sodium acetate; palladium diacetate; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
2: Heck reaction;
DOI:10.1021/ol201983u
