2-[3-[3-(chloromethyl)-5-methylsalicyl]-5-methylsalicyl]-6-(chloromethyl)-4-methylphenol

Base Information

• Chemical Name: 2-[3-[3-(chloromethyl)-5-methylsalicyl]-5-methylsalicyl]-6-(chloromethyl)-4-methylphenol
• CAS No.: 273755-70-7
• Molecular Formula: C₂₅H₂₆Cl₂O₃
• Molecular Weight: 445.386

Synonyms:2-[3-[3-(chloromethyl)-5-methylsalicyl]-5-methylsalicyl]-6-(chloromethyl)-4-methylphenol

Chemical Property of 2-[3-[3-(chloromethyl)-5-methylsalicyl]-5-methylsalicyl]-6-(chloromethyl)-4-methylphenol

Chemical Property:

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Technology Process of 2-[3-[3-(chloromethyl)-5-methylsalicyl]-5-methylsalicyl]-6-(chloromethyl)-4-methylphenol

There total 1 articles about 2-[3-[3-(chloromethyl)-5-methylsalicyl]-5-methylsalicyl]-6-(chloromethyl)-4-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3-[3-[3-(hydroxymethyl)-5-methylsalicyl]-5-methylsalicyl]-2-hydroxy-5-methylbenzylalcohol (22247-59-2) → 2-[3-[3-(chloromethyl)-5-methylsalicyl]-5-methylsalicyl]-6-(chloromethyl)-4-methylphenol (273755-70-7)

Guidance literature:

With thionyl chloride; In benzene; at 20 ℃; for 3h;

DOI:10.1080/00397910008087137

Reference yield: 26.0%

2-[3-[3-(chloromethyl)-5-methylsalicyl]-5-methylsalicyl]-6-(chloromethyl)-4-methylphenol (273755-70-7) + NH=Pro-Phe-Cys(OMe)-SS-Cys(OMe)-Phe-Pro=NH → C61H72N6O11S2

Guidance literature:

With triethylamine; In dichloromethane; at 30 ℃; for 20h;

DOI:10.1248/cpb.50.432

Reference yield: 10.0%

2-[3-[3-(chloromethyl)-5-methylsalicyl]-5-methylsalicyl]-6-(chloromethyl)-4-methylphenol (273755-70-7) + (S)-2-((S)-2-Amino-3-phenyl-propionylamino)-3-[(S)-2-((S)-2-amino-3-phenyl-propionylamino)-2-methoxycarbonyl-ethyldisulfanyl]-propionic acid methyl ester; compound with GENERIC INORGANIC NEUTRAL COMPONENT → C76H82N4O12S2

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 30 ℃; for 18h;

DOI:10.1021/jo000738z

upstream raw materials:

3-[3-[3-(hydroxymethyl)-5-methylsalicyl]-5-methylsalicyl]-2-hydroxy-5-methylbenzylalcohol

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