N-ethenyl-N-[2-(5-iodobenzo[d][1,3]dioxol-6-yl)ethyl]-2,3-dimethoxybenzamide

Base Information

Chemical Name:N-ethenyl-N-[2-(5-iodobenzo[d][1,3]dioxol-6-yl)ethyl]-2,3-dimethoxybenzamide
CAS No.:868053-19-4
Molecular Formula:C₂₀H₂₀INO₅
Molecular Weight:481.287
Hs Code.:

Synonyms:N-ethenyl-N-[2-(5-iodobenzo[d][1,3]dioxol-6-yl)ethyl]-2,3-dimethoxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-ethenyl-N-[2-(5-iodobenzo[d][1,3]dioxol-6-yl)ethyl]-2,3-dimethoxybenzamide

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Technology Process of N-ethenyl-N-[2-(5-iodobenzo[d][1,3]dioxol-6-yl)ethyl]-2,3-dimethoxybenzamide

There total 1 articles about N-ethenyl-N-[2-(5-iodobenzo[d][1,3]dioxol-6-yl)ethyl]-2,3-dimethoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 75-07-0,9002-91-9
acetaldehyde

: 66384-44-9
2-(2-iodo-4,5-methylenedioxyphenyl)ethylamine

: 7169-06-4
2,3-dimethoxybenzoyl chloride

: 868053-19-4
N-ethenyl-N-[2-(5-iodobenzo[d][1,3]dioxol-6-yl)ethyl]-2,3-dimethoxybenzamide

Guidance literature:: acetaldehyde; 2-(2-iodo-4,5-methylenedioxyphenyl)ethylamine; In tetrahydrofuran; at -10 ℃; for 5h;

2,3-dimethoxybenzoyl chloride; With triethylamine; In tetrahydrofuran; at -10 ℃; for 0.5h;
DOI:10.1021/ol051563o