(S)-2-Amino-4-methyl-pentanoic acid [({(1S,2R,3R,4S,5S,6R)-4-amino-3-[(2R,3R,6S)-3-amino-6-(1-amino-ethyl)-tetrahydro-pyran-2-yloxy]-2,5-dihydroxy-6-methoxy-cyclohexyl}-methyl-carbamoyl)-methyl]-amide; hydrochloride

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Chemical Name:(S)-2-Amino-4-methyl-pentanoic acid [({(1S,2R,3R,4S,5S,6R)-4-amino-3-[(2R,3R,6S)-3-amino-6-(1-amino-ethyl)-tetrahydro-pyran-2-yloxy]-2,5-dihydroxy-6-methoxy-cyclohexyl}-methyl-carbamoyl)-methyl]-amide; hydrochloride
CAS No.:66962-83-2
Molecular Formula:C₂₃H₄₆N₆O₇*4ClH
Molecular Weight:664.498
Hs Code.:

(S)-2-Amino-4-methyl-pentanoic acid [({(1S,2R,3R,4S,5S,6R)-4-amino-3-[(2R,3R,6S)-3-amino-6-(1-amino-ethyl)-tetrahydro-pyran-2-yloxy]-2,5-dihydroxy-6-methoxy-cyclohexyl}-methyl-carbamoyl)-methyl]-amide; hydrochloride

Synonyms:(S)-2-Amino-4-methyl-pentanoic acid [({(1S,2R,3R,4S,5S,6R)-4-amino-3-[(2R,3R,6S)-3-amino-6-(1-amino-ethyl)-tetrahydro-pyran-2-yloxy]-2,5-dihydroxy-6-methoxy-cyclohexyl}-methyl-carbamoyl)-methyl]-amide; hydrochloride

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Chemical Property of (S)-2-Amino-4-methyl-pentanoic acid [({(1S,2R,3R,4S,5S,6R)-4-amino-3-[(2R,3R,6S)-3-amino-6-(1-amino-ethyl)-tetrahydro-pyran-2-yloxy]-2,5-dihydroxy-6-methoxy-cyclohexyl}-methyl-carbamoyl)-methyl]-amide; hydrochloride

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Technology Process of (S)-2-Amino-4-methyl-pentanoic acid [({(1S,2R,3R,4S,5S,6R)-4-amino-3-[(2R,3R,6S)-3-amino-6-(1-amino-ethyl)-tetrahydro-pyran-2-yloxy]-2,5-dihydroxy-6-methoxy-cyclohexyl}-methyl-carbamoyl)-methyl]-amide; hydrochloride

There total 5 articles about (S)-2-Amino-4-methyl-pentanoic acid [({(1S,2R,3R,4S,5S,6R)-4-amino-3-[(2R,3R,6S)-3-amino-6-(1-amino-ethyl)-tetrahydro-pyran-2-yloxy]-2,5-dihydroxy-6-methoxy-cyclohexyl}-methyl-carbamoyl)-methyl]-amide; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66962-67-2
C₅₅H₇₀N₆O₁₅

: 66962-83-2
(S)-2-Amino-4-methyl-pentanoic acid [({(1S,2R,3R,4S,5S,6R)-4-amino-3-[(2R,3R,6S)-3-amino-6-(1-amino-ethyl)-tetrahydro-pyran-2-yloxy]-2,5-dihydroxy-6-methoxy-cyclohexyl}-methyl-carbamoyl)-methyl]-amide; hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; for 4h; under 2280 Torr;
DOI:10.1016/S0008-6215(00)85134-4

Reference yield:

: 66962-55-8,71658-13-4,76822-42-9,78609-41-3,78781-05-2
1,2',6'-tri-N-(benzyloxycarbonyl)fortimicin B

: 66962-83-2
(S)-2-Amino-4-methyl-pentanoic acid [({(1S,2R,3R,4S,5S,6R)-4-amino-3-[(2R,3R,6S)-3-amino-6-(1-amino-ethyl)-tetrahydro-pyran-2-yloxy]-2,5-dihydroxy-6-methoxy-cyclohexyl}-methyl-carbamoyl)-methyl]-amide; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / tetrahydrofuran; dioxane / 48 h / Ambient temperature

2: H₂, 0.2 M HCl / 5 percent Pd/C / methanol / 4 h / 2280 Torr

With hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1016/S0008-6215(00)85134-4

Reference yield:

: 66962-56-9,71564-63-1,71873-76-2,73285-02-6,74742-44-2,76822-43-0,79703-12-1
1,2',6',2''-tetra-N-benzyloxycarbonyl-4-N-methyl-fortimicin A

: 66962-83-2
(S)-2-Amino-4-methyl-pentanoic acid [({(1S,2R,3R,4S,5S,6R)-4-amino-3-[(2R,3R,6S)-3-amino-6-(1-amino-ethyl)-tetrahydro-pyran-2-yloxy]-2,5-dihydroxy-6-methoxy-cyclohexyl}-methyl-carbamoyl)-methyl]-amide; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 0.165 g / 5 percent aq. NaHCO₃ / methanol / 4 h / Heating

2: 91 percent / tetrahydrofuran; dioxane / 48 h / Ambient temperature

3: H₂, 0.2 M HCl / 5 percent Pd/C / methanol / 4 h / 2280 Torr

With hydrogenchloride; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1016/S0008-6215(00)85134-4