tert-butyl{[(E)-3-chloro-3-[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-en-1-yl]oxy}diphenylsilane

Base Information

• Chemical Name: tert-butyl{[(E)-3-chloro-3-[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-en-1-yl]oxy}diphenylsilane
• CAS No.: 1092695-73-2
• Molecular Formula: C₂₄H₃₁ClO₃Si
• Molecular Weight: 431.047

Synonyms:tert-butyl{[(E)-3-chloro-3-[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-en-1-yl]oxy}diphenylsilane

Chemical Property of tert-butyl{[(E)-3-chloro-3-[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-en-1-yl]oxy}diphenylsilane

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Technology Process of tert-butyl{[(E)-3-chloro-3-[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-en-1-yl]oxy}diphenylsilane

There total 2 articles about tert-butyl{[(E)-3-chloro-3-[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-en-1-yl]oxy}diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

tert-Butyl-[(2S,3R)-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-oxiranylmethoxy]-diphenyl-silane → tert-butyl{[(E)-3-chloro-3-[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-en-1-yl]oxy}diphenylsilane (1092695-73-2) + tert-butyl{[(E)-2-chloro-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-en-1-yl]oxy}diphenylsilane (1092695-74-3) + tert-butyl[(2R,3R)-2,3-dichloro-3-[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]propoxy]diphenylsilane (1092695-72-1)

Guidance literature:

With N-chloro-succinimide; triphenylphosphine; In toluene; at 90 ℃; for 1h; stereospecific reaction;

DOI:10.1021/jo802093d

Reference yield:

C24H32O4Si (1092695-98-1) → tert-butyl{[(E)-3-chloro-3-[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-en-1-yl]oxy}diphenylsilane (1092695-73-2) + tert-butyl{[(E)-2-chloro-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-en-1-yl]oxy}diphenylsilane (1092695-74-3) + tert-butyl[(2S,3R)-2,3-dichloro-3-[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]propoxy]diphenylsilane (1092695-76-5) + tert-butyl[(2S,3S)-2,3-dichloro-3-[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]propoxy]diphenylsilane (1092695-75-4)

Guidance literature:

With N-chloro-succinimide; triphenylphosphine; In toluene; at 90 ℃; for 2.7h; stereoselective reaction;

DOI:10.1021/jo802093d

upstream raw materials:

C₂₄H₃₂O₄Si

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