sodium salt of N-(2-furylmethyl)-4-phenylthio-5-sulfamoyl-orthanilic acid

Base Information

Chemical Name:sodium salt of N-(2-furylmethyl)-4-phenylthio-5-sulfamoyl-orthanilic acid
CAS No.:69156-08-7
Molecular Formula:C₁₇H₁₅N₂O₆S₃*Na
Molecular Weight:462.504
Hs Code.:

Synonyms:sodium salt of N-(2-furylmethyl)-4-phenylthio-5-sulfamoyl-orthanilic acid

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Chemical Property of sodium salt of N-(2-furylmethyl)-4-phenylthio-5-sulfamoyl-orthanilic acid

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Technology Process of sodium salt of N-(2-furylmethyl)-4-phenylthio-5-sulfamoyl-orthanilic acid

There total 7 articles about sodium salt of N-(2-furylmethyl)-4-phenylthio-5-sulfamoyl-orthanilic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 344880-10-0
2-[(Furan-2-ylmethyl)-amino]-4-phenylsulfanyl-5-sulfamoyl-benzenesulfonic acid phenyl ester

: 69156-08-7
sodium salt of N-(2-furylmethyl)-4-phenylthio-5-sulfamoyl-orthanilic acid

Guidance literature:: With sodium hydroxide; for 1h;
DOI:10.1021/jm00362a017

Reference yield:

: 61791-73-9
4,6-dichlorobenzene-1,3-disulfonyl chloride

: 69156-08-7
sodium salt of N-(2-furylmethyl)-4-phenylthio-5-sulfamoyl-orthanilic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NH₃ / 1.) THF, 5-10 deg C, 2 h, 2.) MeOH, a) reflux, 10 min, b) RT, overnight

2: K₂CO₃ / dimethylformamide / 1 h / 115 °C

3: 1.5 h / 90 °C

4: 83 percent / aq. NaOH / 1 h

With sodium hydroxide; ammonia; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00362a017

Reference yield:

: 108-98-5
thiophenol

: 69156-08-7
sodium salt of N-(2-furylmethyl)-4-phenylthio-5-sulfamoyl-orthanilic acid

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide / 1 h / 115 °C

2: 1.5 h / 90 °C

3: 83 percent / aq. NaOH / 1 h

With sodium hydroxide; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00362a017