C₄₅H₆₀O₁₂Si

Base Information

Chemical Name:C₄₅H₆₀O₁₂Si
CAS No.:153145-52-9
Molecular Formula:C₄₅H₆₀O₁₂Si
Molecular Weight:821.05
Hs Code.:

C<sub>45</sub>H<sub>60</sub>O<sub>12</sub>Si

Synonyms:C₄₅H₆₀O₁₂Si

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Chemical Property of C₄₅H₆₀O₁₂Si

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Technology Process of C₄₅H₆₀O₁₂Si

There total 24 articles about C₄₅H₆₀O₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153145-26-7
C₃₂H₅₆O₇Si₂

: 153145-52-9
C₄₅H₆₀O₁₂Si

Guidance literature:: Multi-step reaction with 13 steps

1: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

2: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

3: 95 percent / CH₂Cl₂ / 15 h / -45 °C

4: 63 percent / Burgess' reagent

5: 100 percent / pyridine

6: 65 percent / OsO₄

7: DBU / toluene / 2 h / 105 °C

8: 75 percent / pyridine, DMAP / 24 h / 25 °C

9: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

10: tetrahydrofuran / 0.17 h / -78 °C

11: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

12: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

13: pyridine, DMAP / 20 h / 25 °C

With pyridine; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;

Reference yield:

: 153145-20-1
C₃₄H₅₈O₇Si₂

: 153145-52-9
C₄₅H₆₀O₁₂Si

Guidance literature:: Multi-step reaction with 20 steps

1: O₃

2: KMnO₄, KH₂PO₄

4: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

5: 100 percent / p-TsOH

6: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

7: acid

8: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

9: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

10: 95 percent / CH₂Cl₂ / 15 h / -45 °C

11: 63 percent / Burgess' reagent

12: 100 percent / pyridine

13: 65 percent / OsO₄

14: DBU / toluene / 2 h / 105 °C

15: 75 percent / pyridine, DMAP / 24 h / 25 °C

16: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

17: tetrahydrofuran / 0.17 h / -78 °C

18: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

19: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

20: pyridine, DMAP / 20 h / 25 °C

With pyridine; dmap; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; pyridine hydrogenfluoride; ozone; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 153145-56-3
C₃₃H₅₆O₈Si₂

: 153145-52-9
C₄₅H₆₀O₁₂Si

Guidance literature:: Multi-step reaction with 19 steps

1: KMnO₄, KH₂PO₄

3: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

4: 100 percent / p-TsOH

5: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

6: acid

7: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

8: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

9: 95 percent / CH₂Cl₂ / 15 h / -45 °C

10: 63 percent / Burgess' reagent

11: 100 percent / pyridine

12: 65 percent / OsO₄

13: DBU / toluene / 2 h / 105 °C

14: 75 percent / pyridine, DMAP / 24 h / 25 °C

15: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

16: tetrahydrofuran / 0.17 h / -78 °C

17: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

18: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

19: pyridine, DMAP / 20 h / 25 °C

With pyridine; dmap; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;