(2S,3aS,7a5)-octahydroindole-2-carboxylic acid p-nitrobenzylic ester p-toluenesulfonate

Base Information

Chemical Name:(2S,3aS,7a5)-octahydroindole-2-carboxylic acid p-nitrobenzylic ester p-toluenesulfonate
CAS No.:959984-64-6
Molecular Formula:C₇H₈O₃S*C₁₆H₂₀N₂O₄
Molecular Weight:476.551
Hs Code.:

Synonyms:(2S,3aS,7a5)-octahydroindole-2-carboxylic acid p-nitrobenzylic ester p-toluenesulfonate

Suppliers and Price of (2S,3aS,7a5)-octahydroindole-2-carboxylic acid p-nitrobenzylic ester p-toluenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3aS,7a5)-octahydroindole-2-carboxylic acid p-nitrobenzylic ester p-toluenesulfonate

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Technology Process of (2S,3aS,7a5)-octahydroindole-2-carboxylic acid p-nitrobenzylic ester p-toluenesulfonate

There total 1 articles about (2S,3aS,7a5)-octahydroindole-2-carboxylic acid p-nitrobenzylic ester p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 619-73-8
4-nitrobenzyl chloride

: 80875-98-5,2055118-14-2
(2S,3aS,7aS)-perhydroindole-2-carboxylic acid

: 104-15-4
toluene-4-sulfonic acid

: 959984-64-6
(2S,3aS,7a5)-octahydroindole-2-carboxylic acid p-nitrobenzylic ester p-toluenesulfonate

Guidance literature:: In toluene; for 3h; Heating / reflux;

Reference yield: 80.0%

: 959984-64-6
(2S,3aS,7a5)-octahydroindole-2-carboxylic acid p-nitrobenzylic ester p-toluenesulfonate

: 82834-12-6
N-<1(S)-(ethoxycarbonyl)butyl>-L-alanine

: 866430-96-8
(2S,3aS,7aS)-1-{2-[1-ethoxycarbonyl-(S)-butylamino]-(S)-propionyl}-octahydroindole-2-carboxylic acid p-nitrobenzylic ester

Guidance literature:: (2S,3aS,7a5)-octahydroindole-2-carboxylic acid p-nitrobenzylic ester p-toluenesulfonate; N-<1(S)-(ethoxycarbonyl)butyl>-L-alanine; With benzotriazol-1-ol; triethylamine; In dichloromethane; at 20 ℃; for 0.25h;

With dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 5h;

With sodium hydrogencarbonate; In water;