2-<(4H-3,1-Benzoxazin-4-one-2-yl)imino>-6-<(p-nitrophenyl)thio>benzthiazol

Base Information

Chemical Name:2-<(4H-3,1-Benzoxazin-4-one-2-yl)imino>-6-<(p-nitrophenyl)thio>benzthiazol
CAS No.:129166-00-3
Molecular Formula:C₂₁H₁₂N₄O₆S₂
Molecular Weight:480.481
Hs Code.:

Synonyms:2-<(4H-3,1-Benzoxazin-4-one-2-yl)imino>-6-<(p-nitrophenyl)thio>benzthiazol

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Chemical Property of 2-<(4H-3,1-Benzoxazin-4-one-2-yl)imino>-6-<(p-nitrophenyl)thio>benzthiazol

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Technology Process of 2-<(4H-3,1-Benzoxazin-4-one-2-yl)imino>-6-<(p-nitrophenyl)thio>benzthiazol

There total 3 articles about 2-<(4H-3,1-Benzoxazin-4-one-2-yl)imino>-6-<(p-nitrophenyl)thio>benzthiazol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 129165-96-4
2-(4H-3,1-Benzoxazin-4-on-2-yl)imino-6-<(p-nitrophenyl)thio>benzthiazol

: 129166-00-3
2-<(4H-3,1-Benzoxazin-4-one-2-yl)imino>-6-<(p-nitrophenyl)thio>benzthiazol

Guidance literature:: With dihydrogen peroxide; In acetic acid; for 48h; Ambient temperature;

Reference yield:

: 129165-93-1
2-(Dimethyldithiocarbamate)-6-<(p-nitrophenyl)thio>benzthiazol

: 129166-00-3
2-<(4H-3,1-Benzoxazin-4-one-2-yl)imino>-6-<(p-nitrophenyl)thio>benzthiazol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / aq. KOH / dimethylformamide / 5 h / Heating

2: 76 percent / 30percent H₂O₂ / acetic acid / 48 h / Ambient temperature

With potassium hydroxide; dihydrogen peroxide; In acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 129166-00-3
2-<(4H-3,1-Benzoxazin-4-one-2-yl)imino>-6-<(p-nitrophenyl)thio>benzthiazol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / aq. KOH / dimethylformamide / 5 h / Heating

2: 76 percent / 30percent H₂O₂ / acetic acid / 48 h / Ambient temperature

With potassium hydroxide; dihydrogen peroxide; In acetic acid; N,N-dimethyl-formamide;