5-phenyl UDP-α-D-galactose

Base Information

• Chemical Name: 5-phenyl UDP-α-D-galactose
• CAS No.: 1242712-28-2
• Molecular Formula: C₂₁H₂₈N₂O₁₇P₂
• Molecular Weight: 642.404
• Mol file: 1242712-28-2.mol

Synonyms:5-phenyl UDP-α-D-galactose

Chemical Property of 5-phenyl UDP-α-D-galactose

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-phenyl UDP-α-D-galactose

There total 6 articles about 5-phenyl UDP-α-D-galactose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-iodouridine-5'-diphosphate-α-D-galactose (1253736-62-7) + phenylboronic acid (98-80-6) → 5-phenyl UDP-α-D-galactose (1242712-28-2)

Guidance literature:

DOI:10.1002/cbic.201000013

Reference yield:

uridine (58-96-8) → 5-phenyl UDP-α-D-galactose (1242712-28-2)

Guidance literature:

Multi-step reaction with 5 steps

1.1: nitric acid; iodine / chloroform / 5 h / 80 °C

2.1: trichlorophosphate / acetonitrile / -5 °C / Inert atmosphere

3.1: dimethyl sulfoxide / 20 °C

3.2: 1.08 h / 20 °C

4.2: 20 °C / Inert atmosphere

5.1: caesium carbonate; water / sodium tetrachloropalladate(II) / 50 °C / Inert atmosphere

With water; iodine; nitric acid; caesium carbonate; trichlorophosphate; sodium tetrachloropalladate(II); In chloroform; dimethyl sulfoxide; acetonitrile;

Reference yield:

5-iodouridine-5′-monophosphate (21016-94-4,7531-46-6) → 5-phenyl UDP-α-D-galactose (1242712-28-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dimethyl sulfoxide / 20 °C

1.2: 1.08 h / 20 °C

2.2: 20 °C / Inert atmosphere

3.1: caesium carbonate; water / sodium tetrachloropalladate(II) / 50 °C / Inert atmosphere

With water; caesium carbonate; sodium tetrachloropalladate(II); In dimethyl sulfoxide;

upstream raw materials:

5-iodouridine-5'-diphosphate-α-D-galactose

phenylboronic acid

uridine

5-iodouridine