C₄₀H₆₈N₂O₅Si

Base Information

• Chemical Name: C₄₀H₆₈N₂O₅Si
• CAS No.: 899421-91-1
• Molecular Formula: C₄₀H₆₈N₂O₅Si
• Molecular Weight: 685.076
• Mol file: 899421-91-1.mol

Synonyms:C₄₀H₆₈N₂O₅Si

Chemical Property of C₄₀H₆₈N₂O₅Si

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₄₀H₆₈N₂O₅Si

There total 1 articles about C₄₀H₆₈N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C30H48N2O4 (848731-55-5) + 4-(tert-butyldimethylsilanyloxy)butanal (87184-81-4) → C40H68N2O5Si (899421-91-1)

Guidance literature:

In benzene; at 80 ℃; for 2h;

DOI:10.1021/ja074300t

Reference yield: 71.0%

C40H68N2O5Si (899421-91-1) → (CH2)10CCH2OCH(CH2)3O((C(CH3)3)(CH3)2Si)(CH2CHCH2NCCHCH)CH2CH2NCH(OCH2C6H4OCH3)CHO (899421-92-2)

Guidance literature:

With 2-iodoxybenzoic aid; In dimethyl sulfoxide; at 23 ℃; for 1.75h;

DOI:10.1021/ja074300t

Reference yield:

C40H68N2O5Si (899421-91-1) → C46H72N2O4Si

Guidance literature:

Multi-step reaction with 4 steps

1: iodoxybenzoic acid / dimethylsulfoxide

2: iBu₂AlH / toluene / -78 - 0 °C

3: Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 0 °C

With diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; dimethyl sulfoxide; toluene;

DOI:10.1002/anie.200600417

upstream raw materials:

C₃₀H₄₈N₂O₄

4-(tert-butyldimethylsilanyloxy)butanal

Downstream raw materials:

(CH₂)10CCH₂OCH(CH₂)3O((C(CH₃)3)(CH₃)2Si)(CH₂CHCH₂NCCHCH)CH₂CH₂NCH(OCH₂C₆H₄OCH₃)CHO