C₂₄H₃₄O₅

Base Information

• Chemical Name: C₂₄H₃₄O₅
• CAS No.: 940939-77-5
• Molecular Formula: C₂₄H₃₄O₅
• Molecular Weight: 402.531
• Mol file: 940939-77-5.mol

Synonyms:C₂₄H₃₄O₅

Chemical Property of C₂₄H₃₄O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₃₄O₅

There total 4 articles about C₂₄H₃₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C16H26O4 (940939-76-4) + p-Methoxybenzyl bromide (2746-25-0) → C24H34O5 (940939-77-5)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; at 0 ℃;

DOI:10.1016/j.tetlet.2007.03.084

Reference yield:

C14H22O4 (940939-74-2) → C24H34O5 (940939-77-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 86 percent / LiAlH₄ / diethyl ether / 1 h / 20 °C

2: 66 percent / propionic acid / xylene / 3 h / 140 °C

3: 93 percent / LDA / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; propionic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; xylene; 1: Claisen rearrangement / 2: orthoester Claisen rearrangement;

DOI:10.1016/j.tetlet.2007.03.084

Reference yield:

C12H20O3 (940939-75-3) → C24H34O5 (940939-77-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 66 percent / propionic acid / xylene / 3 h / 140 °C

2: 93 percent / LDA / tetrahydrofuran / 0 °C

With propionic acid; lithium diisopropyl amide; In tetrahydrofuran; xylene; 1: orthoester Claisen rearrangement;

DOI:10.1016/j.tetlet.2007.03.084

upstream raw materials:

C₁₆H₂₆O₄

p-Methoxybenzyl bromide

C₁₄H₂₂O₄

C₁₂H₂₀O₃

Downstream raw materials:

C₂₂H₃₀O₄