2-azido-5-cyanophenyl iodide

Base Information

• Chemical Name: 2-azido-5-cyanophenyl iodide
• CAS No.: 1030861-82-5
• Molecular Formula: C₇H₃IN₄
• Molecular Weight: 270.032

Synonyms:2-azido-5-cyanophenyl iodide

Chemical Property of 2-azido-5-cyanophenyl iodide

Chemical Property:

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Technology Process of 2-azido-5-cyanophenyl iodide

There total 1 articles about 2-azido-5-cyanophenyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4-amino-3-iodobenzonitrile (33348-34-4) → 2-azido-5-cyanophenyl iodide (1030861-82-5)

Guidance literature:

With tert.-butylnitrite; trimethylsilylazide; In acetonitrile; at 0 - 20 ℃;

DOI:10.1021/ol800675u

Reference yield: 86.0%

2-azido-5-cyanophenyl iodide (1030861-82-5) + 2-(trimethylsilyl)phenyl trifluoromethanesulfonate (88284-48-4) → 4-(1H-benzo[d][1,2,3]triazol-1-yl)-3-iodobenzonitrile (1030862-06-6)

Guidance literature:

With cesium fluoride; In acetonitrile; at 20 ℃; for 18h;

DOI:10.1021/ol800675u

Reference yield: 82.0%

2-azido-5-cyanophenyl iodide (1030861-82-5) + 1-t-Butoxycarbonylpiperazine (57260-71-6) → tert-butyl 4-(2-azido-5-cyanophenyl)piperazine-1-carboxylate

Guidance literature:

With CPhos Pd G₄; sodium t-butanolate; In 1,4-dioxane; at 50 ℃; for 12h; Inert atmosphere;

DOI:10.1021/acs.joc.1c02251

upstream raw materials:

4-amino-3-iodobenzonitrile

Downstream raw materials:

4-(1H-benzo[d][1,2,3]triazol-1-yl)-3-iodobenzonitrile

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