ethyl (E,E)-2-{[2-(tert-butoxycarbonylamino)benzylidene]amino}cinnamate

Base Information

Chemical Name:ethyl (E,E)-2-{[2-(tert-butoxycarbonylamino)benzylidene]amino}cinnamate
CAS No.:1126638-85-4
Molecular Formula:C₂₃H₂₆N₂O₄
Molecular Weight:394.47
Hs Code.:

Synonyms:ethyl (E,E)-2-{[2-(tert-butoxycarbonylamino)benzylidene]amino}cinnamate

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Chemical Property of ethyl (E,E)-2-{[2-(tert-butoxycarbonylamino)benzylidene]amino}cinnamate

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Technology Process of ethyl (E,E)-2-{[2-(tert-butoxycarbonylamino)benzylidene]amino}cinnamate

There total 2 articles about ethyl (E,E)-2-{[2-(tert-butoxycarbonylamino)benzylidene]amino}cinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1126638-83-2
ethyl (E)-2-({[2-(tert-butoxycarbonylamino)phenyl]cyanomethyl}amino)cinnamate

: 1126638-85-4
ethyl (E,E)-2-{[2-(tert-butoxycarbonylamino)benzylidene]amino}cinnamate

: 1126638-84-3
ethyl {2-[2-(tert-butoxycarbonylamino)phenyl]-1H-indol-3-yl}acetate

Guidance literature:: With potassium tert-butylate; In ethanol; at 20 ℃; for 0.5h;
DOI:10.1055/s-0028-1083250

Reference yield:

: potassium cyanide

: 58106-56-2,79655-96-2
ethyl (E)-3-(2-aminophenyl)acrylate

: 74965-38-1
tert-butyl (2-formylphenyl)carbamate

: 1126638-85-4
ethyl (E,E)-2-{[2-(tert-butoxycarbonylamino)benzylidene]amino}cinnamate

: 1126638-84-3
ethyl {2-[2-(tert-butoxycarbonylamino)phenyl]-1H-indol-3-yl}acetate

: 1126638-83-2
ethyl (E)-2-({[2-(tert-butoxycarbonylamino)phenyl]cyanomethyl}amino)cinnamate

Guidance literature:: ethyl (E)-3-(2-aminophenyl)acrylate; tert-butyl (2-formylphenyl)carbamate; With acetic acid; In ethanol; at 50 ℃; for 3h;

potassium cyanide; With acetic acid; In ethanol; at 60 ℃; for 23h;
DOI:10.1055/s-0028-1083250