5-fluoro-4-iodo-2-methoxybenzonitrile

Base Information

Chemical Name:5-fluoro-4-iodo-2-methoxybenzonitrile
CAS No.:431942-70-0
Molecular Formula:C₈H₅FINO
Molecular Weight:277.037
Hs Code.:

Synonyms:5-fluoro-4-iodo-2-methoxybenzonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-fluoro-4-iodo-2-methoxybenzonitrile

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Technology Process of 5-fluoro-4-iodo-2-methoxybenzonitrile

There total 2 articles about 5-fluoro-4-iodo-2-methoxybenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₇BFNO₃

: 431942-70-0
5-fluoro-4-iodo-2-methoxybenzonitrile

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; potassium iodide; In methanol; water; at 80 ℃; for 1h; High pressure;
DOI:10.1021/ol303164h

Reference yield:

: 189628-38-4
5-fluoro-2-methoxybenzonitrile

: 431942-70-0
5-fluoro-4-iodo-2-methoxybenzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4′-di-(tert-butyl)-2,2′-bipyridyl / tetrahydrofuran / 24 h / 80 °C / High pressure; Inert atmosphere

2: 1,10-Phenanthroline; copper(l) iodide; potassium iodide / methanol; water / 1 h / 80 °C / High pressure

With copper(l) iodide; 1,10-Phenanthroline; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4′-di-(tert-butyl)-2,2′-bipyridyl; potassium iodide; In tetrahydrofuran; methanol; water;
DOI:10.1021/ol303164h