N-(5-aminopentyl)-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

Base Information

Chemical Name:N-(5-aminopentyl)-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid
CAS No.:112139-64-7
Molecular Formula:C₃₀H₄₄N₄O₅
Molecular Weight:540.703
Hs Code.:

Synonyms:N-(5-aminopentyl)-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

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Chemical Property of N-(5-aminopentyl)-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

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Technology Process of N-(5-aminopentyl)-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

There total 14 articles about N-(5-aminopentyl)-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 112139-63-6
N-(4-cyanobutyl)-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

: 112139-64-7
N-(5-aminopentyl)-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

Guidance literature:: With ammonia; hydrogen; nickel; In methanol; water; for 2.5h; under 2585.7 Torr;
DOI:10.1021/jo00249a001

Reference yield:

: 83966-23-8
1-Amino-5-pentane

: 112139-64-7
N-(5-aminopentyl)-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / DCC, DMAP / CHCl₃ / 24.5 h / 0 - 20 °C

2: 82 percent / H₂, NH₃ / Raney Ni / methanol; H₂O / 2.5 h / 2585.7 Torr

With dmap; ammonia; hydrogen; dicyclohexyl-carbodiimide; nickel; In methanol; chloroform; water;
DOI:10.1021/jo00249a001

Reference yield:

: 5-[(E)-Benzyloxyimino]-pentanenitrile

: 112139-64-7
N-(5-aminopentyl)-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

Guidance literature:: Multi-step reaction with 4 steps

1: sodium cyanoborohydride, HCl / methanol; H₂O / 3 h / Ambient temperature

2: 98 percent / pyridine / 1.5 h / 100 °C

3: 98 percent / DCC, DMAP / CHCl₃ / 24.5 h / 0 - 20 °C

4: 82 percent / H₂, NH₃ / Raney Ni / methanol; H₂O / 2.5 h / 2585.7 Torr

With pyridine; hydrogenchloride; dmap; ammonia; hydrogen; sodium cyanoborohydride; dicyclohexyl-carbodiimide; nickel; In methanol; chloroform; water;
DOI:10.1021/jo00249a001