methyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Base Information

Chemical Name:methyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside
CAS No.:428865-88-7
Molecular Formula:C₄₄H₄₄Cl₃NO₁₄
Molecular Weight:917.191
Hs Code.:

methyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Synonyms:methyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

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Chemical Property of methyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

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Technology Process of methyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

There total 2 articles about methyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: methyl (methyl 2-O-benzoyl-3-O-benzyl-4-O-chloroacetyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

: 428865-88-7
methyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Guidance literature:: With thiourea; In pyridine; ethanol; at 80 ℃; for 0.666667h;
DOI:10.1002/1099-0690(200203)2002:5<815::AID-EJOC815>3.0.CO;2-A

Reference yield:

: (methyl 2-O-benzoyl-3-O-benzyl-4-O-chloroacetyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-1-O-trichloroacetimidoyl-D-galactopyranose

: 428865-88-7
methyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / TMSOTf; 3A molecular sieves / CH₂Cl₂; toluene / 0.5 h / 20 °C

2: 91 percent / thiourea / pyridine; ethanol / 0.67 h / 80 °C

With trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; thiourea; In pyridine; ethanol; dichloromethane; toluene;
DOI:10.1002/1099-0690(200203)2002:5<815::AID-EJOC815>3.0.CO;2-A

Reference yield: 44.0%

: 428865-88-7
methyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

: (methyl 2-O-benzoyl-3-O-benzyl-4-O-chloroacetyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-1-O-trichloroacetimidoyl-D-galactopyranose

: 428865-89-8
C₈₇H₈₄Cl₆N₂O₂₇

Guidance literature:: methyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside; (methyl 2-O-benzoyl-3-O-benzyl-4-O-chloroacetyl-β-D-glucopyranosyluronate)-(1->3)-6-O-benzoyl-4-O-benzyl-2-deoxy-2-trichloroacetamido-1-O-trichloroacetimidoyl-D-galactopyranose; With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; toluene; at 20 ℃; for 0.5h;

With thiourea; In pyridine; ethanol; at 80 ℃; Further stages.;
DOI:10.1002/1099-0690(200203)2002:5<815::AID-EJOC815>3.0.CO;2-A