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Technology Process of N1,N6-(di-tert-butoxycarbonyl)-N1-(2-methylallyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine

N1,N6-(di-tert-butoxycarbonyl)-N1-(2-methylallyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine

Base Information
  • Chemical Name:N1,N6-(di-tert-butoxycarbonyl)-N1-(2-methylallyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine
  • CAS No.:1228929-81-4
  • Molecular Formula:C29H48N2O6
  • Molecular Weight:520.71
  • Hs Code.:
N<sub>1</sub>,N<sub>6</sub>-(di-tert-butoxycarbonyl)-N<sub>1</sub>-(2-methylallyl)-N<sub>6</sub>-(3,5-dimethoxybenzyl)hexane-1,6-diamine

Synonyms:N1,N6-(di-tert-butoxycarbonyl)-N1-(2-methylallyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine

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Chemical Property of N1,N6-(di-tert-butoxycarbonyl)-N1-(2-methylallyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine
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Technology Process of N1,N6-(di-tert-butoxycarbonyl)-N1-(2-methylallyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine

There total 1 articles about N1,N6-(di-tert-butoxycarbonyl)-N1-(2-methylallyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

2-methyl-3-bromo-1-propene
1458-98-6

2-methyl-3-bromo-1-propene

N<sub>1</sub>,N<sub>6</sub>-(di-tert-butoxycarbonyl)-N<sub>6</sub>-(3,5-dimethoxybenzyl)hexane-1,6-diamine
1228929-79-0

N1,N6-(di-tert-butoxycarbonyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine

N<sub>1</sub>,N<sub>6</sub>-(di-tert-butoxycarbonyl)-N<sub>1</sub>-(2-methylallyl)-N<sub>6</sub>-(3,5-dimethoxybenzyl)hexane-1,6-diamine
1228929-81-4

N1,N6-(di-tert-butoxycarbonyl)-N1-(2-methylallyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine

Guidance literature:
N1,N6-(di-tert-butoxycarbonyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;
With lithium bromide; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 25 ℃; for 0.166667h; Inert atmosphere;
2-methyl-3-bromo-1-propene; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 50 ℃; for 20h; Inert atmosphere;
DOI:10.1021/ol1008119

Reference yield: 81.0%

N<sub>1</sub>,N<sub>6</sub>-(di-tert-butoxycarbonyl)-N<sub>1</sub>-(2-methylallyl)-N<sub>6</sub>-(3,5-dimethoxybenzyl)hexane-1,6-diamine
1228929-81-4

N1,N6-(di-tert-butoxycarbonyl)-N1-(2-methylallyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine

N<sub>1</sub>-(2-methylallyl)-N<sub>6</sub>-(3,5-dimethoxybenzyl)hexane-1,6-diamine dihydrochloride

N1-(2-methylallyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine dihydrochloride

Guidance literature:
With hydrogenchloride; In 1,4-dioxane; at 60 ℃; for 0.166667h;
DOI:10.1021/ol1008119
upstream raw materials:

2-methyl-3-bromo-1-propene

N1,N6-(di-tert-butoxycarbonyl)-N6-(3,5-dimethoxybenzyl)hexane-1,6-diamine

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