(5S)-5-(hydroxymethyl)-1-[3-(5-methoxy-4-methyl-1,3-oxazol-2-yl)propyl]tetrahydro-1H-2-pyrrolone

Base Information

• Chemical Name: (5S)-5-(hydroxymethyl)-1-[3-(5-methoxy-4-methyl-1,3-oxazol-2-yl)propyl]tetrahydro-1H-2-pyrrolone
• CAS No.: 274675-75-1
• Molecular Formula: C₁₃H₂₀N₂O₄
• Molecular Weight: 268.313

Synonyms:(5S)-5-(hydroxymethyl)-1-[3-(5-methoxy-4-methyl-1,3-oxazol-2-yl)propyl]tetrahydro-1H-2-pyrrolone

Chemical Property of (5S)-5-(hydroxymethyl)-1-[3-(5-methoxy-4-methyl-1,3-oxazol-2-yl)propyl]tetrahydro-1H-2-pyrrolone

Chemical Property:

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Technology Process of (5S)-5-(hydroxymethyl)-1-[3-(5-methoxy-4-methyl-1,3-oxazol-2-yl)propyl]tetrahydro-1H-2-pyrrolone

There total 1 articles about (5S)-5-(hydroxymethyl)-1-[3-(5-methoxy-4-methyl-1,3-oxazol-2-yl)propyl]tetrahydro-1H-2-pyrrolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-Pyroglutaminol (17342-08-4) → (5S)-5-(hydroxymethyl)-1-[3-(5-methoxy-4-methyl-1,3-oxazol-2-yl)propyl]tetrahydro-1H-2-pyrrolone (274675-75-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 93 percent / trichloroacetic acid / CHCl₃ / 4 h / 20 °C

2.1: NaH / dimethylformamide / 1 h / 0 °C

2.2: 67 percent / dimethylformamide / 24 h / 70 °C

3.1: 83 percent / p-TsOH; MeOH / 9 h / 20 °C

With methanol; sodium hydride; toluene-4-sulfonic acid; trichloroacetic acid; In chloroform; N,N-dimethyl-formamide; 1.1: Addition / 2.1: Metallation / 2.2: Alkylation / 3.1: deacetalization;

DOI:10.1021/ja994214w

upstream raw materials:

(S)-Pyroglutaminol

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