3-tert-butylamino imidazo[1,2-a]pyridine-6-carboxylic acid 4-(3,5-difluorobenzenesulfonyl)benzylamide

Base Information

Chemical Name:3-tert-butylamino imidazo[1,2-a]pyridine-6-carboxylic acid 4-(3,5-difluorobenzenesulfonyl)benzylamide
CAS No.:1454285-27-8
Molecular Formula:C₂₅H₂₄F₂N₄O₃S
Molecular Weight:498.553
Hs Code.:

Synonyms:3-tert-butylamino imidazo[1,2-a]pyridine-6-carboxylic acid 4-(3,5-difluorobenzenesulfonyl)benzylamide

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Chemical Property of 3-tert-butylamino imidazo[1,2-a]pyridine-6-carboxylic acid 4-(3,5-difluorobenzenesulfonyl)benzylamide

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Technology Process of 3-tert-butylamino imidazo[1,2-a]pyridine-6-carboxylic acid 4-(3,5-difluorobenzenesulfonyl)benzylamide

There total 9 articles about 3-tert-butylamino imidazo[1,2-a]pyridine-6-carboxylic acid 4-(3,5-difluorobenzenesulfonyl)benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1448536-61-5
(4-((3,5-difluorophenyl)sulfonyl)phenyl)methanamine

: 1453176-68-5
3-tert-butylamino-imidazo[1,2-a]pyridine-6-carboxylic acid

: 1454285-27-8
3-tert-butylamino imidazo[1,2-a]pyridine-6-carboxylic acid 4-(3,5-difluorobenzenesulfonyl)benzylamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 36052-24-1
methyl 6-aminonicotinoate

: 1454285-27-8
3-tert-butylamino imidazo[1,2-a]pyridine-6-carboxylic acid 4-(3,5-difluorobenzenesulfonyl)benzylamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: perchloric acid / methanol / 0.5 h

1.2: 12 h / 20 °C

2.1: sodium hydroxide / water; methanol / 1.5 h / 46 °C

3.1: acetic acid

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 20 °C

With perchloric acid; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 1454285-27-8
3-tert-butylamino imidazo[1,2-a]pyridine-6-carboxylic acid 4-(3,5-difluorobenzenesulfonyl)benzylamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: perchloric acid / methanol / 0.5 h

1.2: 12 h / 20 °C

2.1: sodium hydroxide / water; methanol / 1.5 h / 46 °C

3.1: acetic acid

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 20 °C

With perchloric acid; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In methanol; water; N,N-dimethyl-formamide;