(5S,6S)-5-(1-ethoxyethoxy)-1-(furan-2-yl)-7-(4-methoxybenzyloxy)-6-methylhept-2-yn-1-one

Base Information

Chemical Name:(5S,6S)-5-(1-ethoxyethoxy)-1-(furan-2-yl)-7-(4-methoxybenzyloxy)-6-methylhept-2-yn-1-one
CAS No.:1208114-18-4
Molecular Formula:C₂₄H₃₀O₆
Molecular Weight:414.499
Hs Code.:

Synonyms:(5S,6S)-5-(1-ethoxyethoxy)-1-(furan-2-yl)-7-(4-methoxybenzyloxy)-6-methylhept-2-yn-1-one

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Chemical Property of (5S,6S)-5-(1-ethoxyethoxy)-1-(furan-2-yl)-7-(4-methoxybenzyloxy)-6-methylhept-2-yn-1-one

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Technology Process of (5S,6S)-5-(1-ethoxyethoxy)-1-(furan-2-yl)-7-(4-methoxybenzyloxy)-6-methylhept-2-yn-1-one

There total 1 articles about (5S,6S)-5-(1-ethoxyethoxy)-1-(furan-2-yl)-7-(4-methoxybenzyloxy)-6-methylhept-2-yn-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 527-69-5
2-furancarbonyl chloride

: 1208114-03-7
1-(((2S,3S)-3-(1-Ethoxyethoxy)-2-methylhex-5-ynyloxy)methyl)-4-methoxybenzene

: 1208114-18-4
(5S,6S)-5-(1-ethoxyethoxy)-1-(furan-2-yl)-7-(4-methoxybenzyloxy)-6-methylhept-2-yn-1-one

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja9097252

Reference yield:

: 1208114-18-4
(5S,6S)-5-(1-ethoxyethoxy)-1-(furan-2-yl)-7-(4-methoxybenzyloxy)-6-methylhept-2-yn-1-one

: 1208114-49-1
(1S,5S,6S)-5-(1-ethoxyethoxy)-1-(furan-2-yl)-7-(4-methoxybenzyloxy)-6-methylhept-2-yn-1-ol

Guidance literature:: With dimethylsulfide borane complex; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; toluene; at -40 - 0 ℃; Molecular sieve;
DOI:10.1021/ja9097252

Reference yield:

: 1208114-18-4
(5S,6S)-5-(1-ethoxyethoxy)-1-(furan-2-yl)-7-(4-methoxybenzyloxy)-6-methylhept-2-yn-1-one

: 1208114-49-1
(1S,5S,6S)-5-(1-ethoxyethoxy)-1-(furan-2-yl)-7-(4-methoxybenzyloxy)-6-methylhept-2-yn-1-ol

: C₂₄H₃₂O₆

Guidance literature:: With dimethylsulfide borane complex; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; at -40 ℃; for 3h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/jo1010203