1-(((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-diphenylmethylimidazolium iodide

Base Information

Chemical Name:1-(((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-diphenylmethylimidazolium iodide
CAS No.:496067-61-9
Molecular Formula:C₃₁H₃₆N₃O*I
Molecular Weight:593.551
Hs Code.:

Synonyms:1-(((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-diphenylmethylimidazolium iodide

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Chemical Property of 1-(((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-diphenylmethylimidazolium iodide

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Technology Process of 1-(((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-diphenylmethylimidazolium iodide

There total 6 articles about 1-(((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-diphenylmethylimidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2094-72-6
1-Adamantanecarbonyl chloride

: 496067-61-9
1-(((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-diphenylmethylimidazolium iodide

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / Et₃N / CH₂Cl₂ / 12 h / 25 °C

2: 60 percent / NaBH₄ / ethanol / 12 h / 25 °C

3: 80 percent / Et₃N / CH₂Cl₂ / 24 h / 0 - 25 °C

4: 89 percent / KI / acetone / 4 h / 56 °C

5: dimethylformamide / 12 h / 80 °C

With sodium tetrahydroborate; triethylamine; potassium iodide; In ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja028142b

Reference yield:

: 91-00-9
Benzhydrylamine

: 496067-61-9
1-(((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-diphenylmethylimidazolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₃PO₄ / H₂O; dioxane / 0.5 h / 80 °C / pH 2

1.2: 28 percent / aq. NH₄Cl / H₂O; dioxane / 3 h / 100 °C

2.1: dimethylformamide / 12 h / 80 °C

With phosphoric acid; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja028142b

Reference yield:

: 496067-58-4
Adamantane-1-carboxylic acid ((S)-3-hydroxy-1-hydroxymethyl-propyl)-amide

: 496067-61-9
1-(((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-diphenylmethylimidazolium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / Et₃N / CH₂Cl₂ / 24 h / 0 - 25 °C

2: 89 percent / KI / acetone / 4 h / 56 °C

3: dimethylformamide / 12 h / 80 °C

With triethylamine; potassium iodide; In dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja028142b