Technology Process of 2-morpholinobenzamide
There total 8 articles about 2-morpholinobenzamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
samarium diiodide;
In
tetrahydrofuran;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/ol203353a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; Trimethylacetic acid / methanol / 16 h / 20 °C / Inert atmosphere
2: samarium diiodide / tetrahydrofuran / 20 °C / Inert atmosphere
With
samarium diiodide; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; Trimethylacetic acid;
In
tetrahydrofuran; methanol;
DOI:10.1021/ol203353a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere
2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; Trimethylacetic acid / methanol / 16 h / 20 °C / Inert atmosphere
3: samarium diiodide / tetrahydrofuran / 20 °C / Inert atmosphere
With
samarium diiodide; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; triethylamine; Trimethylacetic acid;
In
tetrahydrofuran; methanol;
DOI:10.1021/ol203353a
