4-[2-oxo-3-([1,2,4]triazol-4-yliminomethyl)-2H-quinolin-1-ylmethyl]-biphenyl-2-carboxylic acid

Base Information

Chemical Name:4-[2-oxo-3-([1,2,4]triazol-4-yliminomethyl)-2H-quinolin-1-ylmethyl]-biphenyl-2-carboxylic acid
CAS No.:1599479-40-9
Molecular Formula:C₂₆H₁₉N₅O₃
Molecular Weight:449.469
Hs Code.:

Synonyms:4-[2-oxo-3-([1,2,4]triazol-4-yliminomethyl)-2H-quinolin-1-ylmethyl]-biphenyl-2-carboxylic acid

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Chemical Property of 4-[2-oxo-3-([1,2,4]triazol-4-yliminomethyl)-2H-quinolin-1-ylmethyl]-biphenyl-2-carboxylic acid

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Technology Process of 4-[2-oxo-3-([1,2,4]triazol-4-yliminomethyl)-2H-quinolin-1-ylmethyl]-biphenyl-2-carboxylic acid

There total 12 articles about 4-[2-oxo-3-([1,2,4]triazol-4-yliminomethyl)-2H-quinolin-1-ylmethyl]-biphenyl-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.8%

: 584-13-4
4-amino-1,2,4-triazole

: C₂₄H₁₇NO₄

: 1599479-40-9
4-[2-oxo-3-([1,2,4]triazol-4-yliminomethyl)-2H-quinolin-1-ylmethyl]-biphenyl-2-carboxylic acid

Guidance literature:: In methanol; Reflux;
DOI:10.1007/s12039-013-0541-4

Reference yield:

: C₂₇H₂₁N₅O₃

: 1599479-40-9
4-[2-oxo-3-([1,2,4]triazol-4-yliminomethyl)-2H-quinolin-1-ylmethyl]-biphenyl-2-carboxylic acid

Guidance literature:: With water; potassium hydroxide; In methanol; for 2h; Reflux;
DOI:10.1007/s12039-013-0541-4

Reference yield:

: 5720-05-8
4-methylphenylboronic acid

: 1599479-40-9
4-[2-oxo-3-([1,2,4]triazol-4-yliminomethyl)-2H-quinolin-1-ylmethyl]-biphenyl-2-carboxylic acid

Guidance literature:: Multi-step reaction with 6 steps

1: palladium diacetate; triethylamine; triphenylphosphine / acetonitrile

2: Acidic conditions

3: bromine / water

4: potassium carbonate / N,N-dimethyl-formamide / 20 °C

5: potassium hydroxide; water / methanol / 2 h / Reflux

6: methanol / Reflux

With water; bromine; palladium diacetate; potassium carbonate; triethylamine; triphenylphosphine; potassium hydroxide; In methanol; water; N,N-dimethyl-formamide; acetonitrile; 1: |Suzuki Coupling;
DOI:10.1007/s12039-013-0541-4